Reference for z-filter MQ-MAS

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Z-filter MQ-MAS references

Below are provided some NMR references about MQ-MAS with z-filter sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver-phase relationship.

  1. N. Malicki, L. Mafra, A.-A. Quoineaud, J. Rocha, F. Thibault-Starzyk, and C. Fernandez
    Multiplex MQMAS NMR of quadrupolar nuclei, (1)(2)(3)
    Solid State Nucl. Magn. Reson. 28, 13-21 (2005).
  2. C. M. Morais, M. Lopes, C. Fernandez, and J. Rocha
    Assessing the potential of fast amplitude modulation pulses for improving triple-quantum magic angle spinning NMR spectra of half-integer quadrupolar nuclei, (1)(2)
    Magn. Reson. Chem. 41, 679-688 (2003).
  3. David Rovnyak, Claudiu Filip, Boris Itin, Alan S. Stern, Gerhard Wagner, Robert G. Griffin, and Jeffrey C. Hoch
    Multiple-quantum magic-angle spinning spectroscopy using nonlinear sampling, (1)(2)(3)
    J. Magn. Reson. 161, 43-55 (2003).
  4. T. Ohkubo, K. Kanehashi, K. Saito, and Y. Ikeda
    Observation of two 4-coordinated Al sites in montmorillonite using high magnetic field strength 27Al MQMAS NMR, (1)(2)
    Clays Clay Miner. 51, 513-518 (2003).
  5. A. Goldbourt and P. K. Madhu
    Multiple-Quantum Magic Angle Spinning: High-resolution solid state NMR spectroscopy of half-integer quadrupolar nuclei, (1)(2)(3)(4)
    Monatsh. Chem. 133, 1497-1534 (2002).
  6. L. Frydman
    Fundamentals of MQMAS NMR on half-integer quadrupolar nuclei, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 262-274, 2002).
  7. J.-P. Amoureux and M. Pruski
    Advances in MQMAS NMR, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 226-251, 2002).
  8. G. Wu and S. Dong
    Two-dimensional 17O multiple quantum magic-angle spinning NMR of organic solids, (3)
    J. Am. Chem. Soc. 123, 9119-9125 (2001).
  9. S. E. Ashbrook and S. Wimperis
    Novel two-dimensional NMR methods that combine single-quantum cross-polarization and MQ-MAS of quadrupolar nuclei, (1)(2)
    Chem. Phys. Lett. 2001, 500-508 (2001).
  10. D. Freude
    Quadrupolar nuclei in solid-state nuclear magnetic resonance, (1)(2)
    in Encyclopedia of Analytical Chemistry, edited by R. A. Meyers, (J. Wiley, Chichester, 12188-12224, 2000).
  11. K. J. Pike, R. P. Malde, S. E. Ashbrook, J. McManus, and S. Wimperis
    Multiple-quantum MAS NMR of quadrupolar nuclei. Do five-, seven- and nine-quantum experiments yield higher resolution than the three-quantum experiment?, (1)(2)
    Solid State Nucl. Magn. Reson. 16, 203-215 (2000).
  12. S. E. Ashbrook and S. Wimperis
    Multiple-quantum cross-polarization and two-dimensional MQMAS NMR of quadrupolar nuclei, (1)(2)
    J. Magn. Reson. 147, 238-249 (2000).
  13. L. J. Smith, H. Eckert, and A. K. Cheetham
    Site preferences in the mixed cation zeolite, Li,Na-Chabazite: A combined solid-state NMR and neutron diffraction study, (1)(2)
    J. Am. Chem. Soc. 122, 1700-1708 (2000).
  14. M. Pruski, J. W. Wiench, and J.-P. Amoureux
    On the conversion of triple- to single-quantum coherences in MQMAS NMR, (1)(2)
    J. Magn. Reson. 147, 286-295 (2000).
  15. F. Taulelle, M. Pruski, J.-P. Amoureux, D. Lang, A. Bailly, C. Huguenard, M. Haouas, C. Gérardin, T. Loiseau, and G. Ferey
    Isomerization of the prenucleation building unit during crystallization of AlPO4-CJ2: An MQMAS, CP-MQMAS, and HETCOR NMR study, (1)
    J. Am. Chem. Soc. 121, 12148-12153 (1999).
  16. M. E. Smith and E. R. H. van Eck
    Recent advances in experimental solid state NMR methodology for half-integer spin quadrupolar nuclei, (1)(2)
    Progr. Nucl. Magn. Reson. Spectros. 34, 159-201 (1999).
  17. J. C. C. Chan
    High-resolution heteronuclear correlation between quadrupolar nuclei, (1)(3)
    J. Magn. Reson. 140, 487-490 (1999).
  18. J. C. C. Chan, M. Bertmer, and H. Eckert
    Sites connectivities in amorphous materials studied by double-resonance NMR of quadrupolar nuclei: High-resolution 11B<->27Al spectroscopy of aluminoborate glasses, (1)
    J. Am. Chem. Soc. 121, 5238-5248 (1999).
  19. M. Pruski, A. Bailly, D. P. Lang, J.-P. Amoureux, and C. Fernandez
    Studies of heteronuclear dipolar interactions between spin-1/2 and quadrupolar nuclei by using REDOR during multiple quantum evolution, (1)(2)(3)
    Chem. Phys. Lett. 307, 35-40 (1999).
  20. L. Züchner, J. C. C. Chan, W. Müller-Warmuth, and H. Eckert
    Short-range order and site connectivities in sodium aluminoborate glasses: I. Quantification of local environments by high-resolution 11B, 23Na, and 27Al solid-state NMR, (1)(2)
    J. Phys. Chem. B 102, 4495-4506 (1998).
  21. T. Charpentier, C. Fermon, and J. Virlet
    Numerical and theoretical analysis of multiquantum MAS experiments, (1)(2)
    J. Chem. Phys. 109, 3116-3130 (1998).
  22. T. Charpentier and J. Virlet
    3Q MQMAS spectroscopy of 59Co (I = 7/2) in Na3Co(NO2)6 and trans-Co[(en2)(NO2)2]NO3 interplay between the quadrupole coupling and anisotropic shielding tensors, (1)(2)
    Solid State Nucl. Magn. Reson. 12, 227-242 (1998).
  23. M. Hanaya and R. K. Harris
    Two-dimensional 23Na MQ MAS NMR study of layered silicates, (1)
    J. Mater. Chem. 8, 1073-1079 (1998).
  24. C. Fernandez, D. P. Lang, J.-P. Amoureux, and M. Pruski
    Measurement of heteronuclear dipolar interactions between quadrupolar and spin-1/2 nuclei in solids by multiple-quantum REDOR NMR, (1)(2)(3)
    J. Am. Chem. Soc. 120, 2672-2673 (1998).
  25. M. Hanaya and R. K. Harris
    Optimization of 2D MQ-MAS NMR experiments for I = 3/2 nuclei on a moderate-field spectrometer, (1)(2)(3)
    J. Phys. Chem. A 101, 6903-6910 (1997).
  26. S. P. Brown and S. Wimperis
    Two-dimensional MQ-MAS NMR of quadrupolar nuclei: a comparison of methods, (1)(2)(3)
    J. Magn. Reson. 128, 42-61 (1997).
  27. P. J. Dirken, S. C. Kohn, M. E. Smith, and E. R. H. van Eck
    Complete resolution of Si-O-Si and Si-O-Al fragments in an aluminosilicate glass by 17O MQMAS NMR spectroscopy, (1)(2)(3)
    Chem. Phys. Lett. 266, 568-574 (1997).
  28. C. Fernandez, L. Delevoye, J.-P. Amoureux, D. P. Lang, and M. Pruski
    27Al{1H} cross polarization triple-quantum MAS NMR, (1)(3)
    J. Am. Chem. Soc. 119, 6858-6862 (1997).
  29. J.-P. Amoureux, C. Fernandez, and S. Steuernagel
    Z filtering in MQ MAS NMR, (2)
    J. Magn. Reson. A 123, 116-118 (1996).

Related bibliography

  1. Judith Schlagnitweit, Michaela Horničáková, Gerhard Zuckerstätter, and Norbert Müller
    MQD—Multiplex-Quadrature Detection in multi-dimensional NMR,
    ChemPhysChem 13, 342-346 (2012).
    Open access
  2. Z. H. Gan and H. T. Kwak
    Enhancing MQMAS sensitivity using signals from multiple coherence transfer pathways,
    J. Magn. Reson. 168, 346-351 (2004).
  3. T. S. Mahesh, T. G. Ajithkumar, C. S. Nagaraja, G. Bodenhausen, and A. Kumar
    Suppression of sidebands in two-dimensional exchange and MQMAS spectroscopies in solids by variable-speed magic-angle sample spinning,
    Chem. Phys. Lett. 319, 278-282 (2000).
  4. V. Lacassagne, P. Florian, V. Montouillout, C. Gervais, F. Babonneau, and D. Massiot
    Resolution enhancement in solid-state MQ-MAS experiments achieved by composite decoupling,
    Magn. Reson. Chem. 36, 956-959 (1998).

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