Reference for 1Q-CP followed by MQ-MAS

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1Q-CP MQ-MAS references

Below are provided some NMR references for single-quantum Cross- Polarization followed by MQ-MAS sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling.

  1. J.-P. Amoureux and M. Pruski,
    Advances in MQMAS NMR, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 226-251, 2002).
  2. S. E. Ashbrook and S. Wimperis
    Novel two-dimensional NMR methods that combine single-quantum cross-polarization and MQ-MAS of quadrupolar nuclei, (1)(2)
    Chem. Phys. Lett. 2001, 500-508 (2001).
  3. K. H. Lim and C. P. Grey
    19F/23Na multiple quantum cross polarization NMR in solids, (1)(3)
    J. Chem. Phys. 112, 7490-7504 (2000).
  4. S. E. Ashbrook and S. Wimperis
    Multiple-quantum cross-polarization and two-dimensional MQMAS NMR of quadrupolar nuclei, (1)(2)
    J. Magn. Reson. 147, 238-249 (2000).
  5. M. Pruski, C. Fernandez, D. P. Lang, and J.-P. Amoureux
    Measurement of interatomic connectivities in molecular sieves using MQMAS-based methods, (1)(2)
    Catal. Today 49, 401-409 (1999).
  6. F. Taulelle, M. Pruski, J.-P. Amoureux, D. Lang, A. Bailly, C. Huguenard, M. Haouas, C. Gérardin, T. Loiseau, and G. Ferey
    Isomerization of the prenucleation building unit during crystallization of AlPO4-CJ2: An MQMAS, CP-MQMAS, and HETCOR NMR study, (1)(2)
    J. Am. Chem. Soc. 121, 12148-12153 (1999).
  7. C. Fernandez, L. Delevoye, J.-P. Amoureux, D. P. Lang, and M. Pruski
    27Al{1H} cross polarization triple-quantum MAS NMR, (1)(3)
    J. Am. Chem. Soc. 119, 6858-6862 (1997).
  8. M. Pruski, D. P. Lang, C. Fernandez, and J.-P. Amoureux
    MQ MAS NMR with cross-polarization: Spectral editing of high-resolution spectra of quadrupolar nuclei, (1)(2)
    Solid State Nucl. Magn. Reson. 7, 327-331 (1997).

Related bibliography

  1. S. E. Ashbrook and S. Wimperis
    Single- and multiple-quantum cross-polarization in NMR of quadrupolar nuclei in static samples, (1)(2)
    Mol. Phys. 98, 1-26 (2000).
  2. A. J. Vega
    CP/MAS of quadrupolar S = 3/2 nuclei,
    Solid State Nucl. Magn. Reson. 1, 17-32 (1992).

Solid-state NMR bibliography for:

Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91
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