Nutation NMR pulse programs for Avance spectrometers with XwinNMR 3.5 operating system

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AVANCE spectrometers
with xwinnmr 3.5 operating system

SF = BF1 + SR (Larmor frequency of reference sample)

SFO1 = BF1 + O1 (spectrometer frequency)

These pulse programs are available for both 1D and 2D NMR experiments.

amplitude-modulated
experiments


SPAM-echo/antiecho (2D only)

MQMAS data processing:
Shearing the 2D spectrum with AU program xfshear 2005


Z-filter

Cogwheel z-filter for I = 3/2

Definition of echo and antiecho signals

MQMAS data processing:
Shearing the 2D spectrum with AU program xfshear 2001


z-filter ±3QMAS for I = 3/2, 5/2, and 7/2

z-filter ±5QMAS for I = 5/2, 7/2, and 9/2

z-filter ±7QMAS for I = 7/2 and 9/2

z-filter ±9QMAS for I = 9/2


Shifted-echo with 3 strong pulses

Shifted-echo with 3 pulses


Two-pulse

phase-modulated
experiments


Multiplex SPAM (2D only)


Multiplex z-filter (2D only)


Split-t1

Cogwheel split-t1 3QMAS for I = 3/2

Split-t2 with two pulses


Shifted-echo for I = 3/2 with 3 strong pulses

Shifted-echo for I = 3/2 with 3 pulses

Shifted-echo for I > 3/2 with 3 strong pulses

Shifted-echo for I > 3/2 with 3 pulses

Cogwheel shifted-echo 3QMAS for I = 5/2

1-D experiments


  • qcpmgall.av, pulse program which samples continuously, including ALL pulses and ringdown delays
  • au_qcpmg, AU program which takes out data points sampled during pulses and ring down delays.
    If digmod is used, convert data to analog with convdta command.
    ALWAYS use this AU program on a COPY of dataset.
  • qcpmgaddjt from Julien Trébosc, AU program which stores echos from qcpmgall.av pulse program by adding them up.
    Use absolute scale for Y-axis to check the amplitude of echo in the FID window.
    If digmod is used, convert data to analog with convdta command.
    ALWAYS use this AU program on a COPY of dataset.
  • qcpmgsplit, AU program for splitting CPMG echo train acquired with qcpmgall.av pulse program. These echoes allow T2 measurement.

  • hpdecqcpmgall.av, pulse program for performing CPMG experiment with high power decoupling , which samples continuously, including ALL pulses and ringdown delays
  • cpqcpmgall.av, pulse program for performing basic cross-polarisation experiment with CPMG detection, which samples continuously, including ALL pulses and ringdown delays

(top)

Solid-state NMR bibliography for:

Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91
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