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Proton high-power decoupling 29Si MAS QCPMG data of Nanomacs

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Proton high-power decoupling silicon-29 QCPMG echo train of nanomacs with NS = 48

Figure 1: Proton high-power decoupling 29Si MAS QCPMG echo train of nanomacs with NS = 48

Acquisition parameters:

General  
PULPROG hpdeccpmg.fau
TD 1564
NS 48
DS 0
SWH [Hz] 20000.00
AQ [s] 0.0391500
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 1562.572021
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.00200000
L22 9
P25 [µs] 0.00
ZGOPTNS
rest [s] 0.00008570
Channel f1  
NUC1 29Si
P3 [µs] 6.30
P4 [µs] 12.70
PL1 [dB] 6.00
PL1W [W] 130.48197937
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3677143
Channel f2  
CNST21 0.0000000
CPDPRG2 tppm15
NUC2 1H
PCPD2 [µs] 9.90
PL2 [dB] 120.00
PL2W [W] 0.00000000
PL12 [dB] 10.00
PL12W [W] 32.07678986
SFO2 [MHz] 500.2113720

Proton high-power decoupling 29Si MAS QCPMG data of Nanomacs

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Proton high-power decoupling silicon-29 QCPMG echo train of nanomacs with NS = 1200

Figure 2: Proton high-power decoupling 29Si MAS QCPMG echo train of nanomacs with NS = 1200

29Si spikelet spectrum of nanomacs

(a) Spectrum without linebroadening of Figure 1

29Si spikelet spectrum of nanomacs with NS = 48

(b) Spectrum with SVD denoising of Figure 1

SVD 29Si spikelet spectrum of nanomacs with NS = 48

(c) Spectrum without linebroadening of Figure 2

29Si spikelet spectrum of nanomacs with NS = 1200

Solid-state NMR bibliography for:

Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91
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