What's new
Zeolite NaX

Home and Applets > What's New > Zeolite NaX

29Si MAS QCPMG echo train of zeolite LSX

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of LSX zeolite

29Si MAS QCPMG echo train of zeolite LSX

Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 31288
NS 48
DS 0
SWH [Hz] 20000.00
AQ [s] 0.7822500
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 31287.650391
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.02000000
L22 19
P25 [µs] 0.00
rest [s] 0.00005873
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3690980

29Si MAS QCPMG echo train of zeolite NaX

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of NaX zeolite

29Si MAS QCPMG echo train of NaX

Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 4604
NS 336
DS 0
SWH [Hz] 20000.00
AQ [s] 0.1151500
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 4602.572266
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.00600000
L22 9
P25 [µs] 0.00
rest [s] 0.00008569
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3690980

29Si MAS QCPMG echo train of zeolite NaY

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of NaY zeolite

29Si MAS QCPMG echo train of NaY

Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 13468
NS 72
DS 0
SWH [Hz] 20000.00
AQ [s] 0.3367500
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 13466.829102
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.00400000
L22 41
P25 [µs] 0.00
rest [s] 0.00007929
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3685010

29Si MAS QCPMG echo train of zeolite LZY64

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of LZY64 zeolite

29Si MAS QCPMG echo train of LZY64

29Si MAS QCPMG echo train of stabilized zeolite NH4Y, Si/Al = 6

Experiment performed with 4-mm diameter rotor spinning at 10 kHz.

Silicon-29 QCPMG echo train of stabilized NH4Y zeolite, Si/Al = 6

29Si MAS QCPMG echo train of stabilized zeolite NH4Y, Si/Al = 6

Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 13468
NS 288
DS 0
SWH [Hz] 20000.00
AQ [s] 0.3367500
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 13466.829102
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.00400000
L22 41
P25 [µs] 0.00
rest [s] 0.00007929
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3675560

29Si MAS QCPMG echo train of zeolite Beta

Experiment performed with 4-mm diameter rotor spinning at 12 kHz.

Silicon-29 QCPMG echo train of Beta zeolite

29Si MAS QCPMG echo train of zeolite Beta

Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 12818
NS 240
DS 0
SWH [Hz] 20000.00
AQ [s] 0.3205000
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 12817.812500
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.00400000
L22 39
P25 [µs] 0.00
rest [s] 0.00005467
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3669695

29Si MAS QCPMG echo train of zeolite Silicalite

Experiment performed with 4-mm diameter rotor spinning at 12 kHz.

Silicon-29 QCPMG echo train of Silicalite zeolite

29Si MAS QCPMG echo train of zeolite Silicalite

Acquisition parameters:

General  
PULPROG qcpmg.fau
TD 83188
NS 320
DS 0
SWH [Hz] 20000.00
AQ [s] 2.0797501
RG 128
DW [µs] 25.000
DE [µs] 6.50
const1 83186.828125
CONST11 0.0000000
D1 [s] 180.00000000
D3 [s] 0.00005000
D6 [s] 0.02500000
L22 41
P25 [µs] 0.00
rest [s] 0.00007936
Channel f1  
NUC1 29Si
P3 [µs] 6.35
P4 [µs] 12.70
PL1 [dB] 120
PL1W [W] 0.00000000
PL21 [dB] 6.00
PL21W [W] 130.48197937
PL22 [dB] 6.00
PL22W [W] 130.48197937
SFO1 [MHz] 99.3665330

Solid-state NMR bibliography for:

Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91
[Contact me] - Last updated February 16, 2020
Copyright © 2002-2020 pascal-man.com. All rights reserved.