Cross-polarization
交叉極化

Double-resonance
雙頻共振

MQ-MAS
多量子 魔角旋轉

• Two-pulse
• References
• Related
• Simulation
• Pulse program
• Phase cycling
  
• Shifted-echo
• References
• Simulation
• Pulse program
• Phase cycling
  
• Z-filter
• References
• Simulation
• Pulse program
• Phase cycling
  
• SPAM
• References
• Pulse program
• Phase cycling
  
• Split-t1
• References
• Pulse program
  
• Mixed-coherence
• References
  

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• MQ-HETCOR
• References
  
• Correlation
• References
  

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• CP-MQ
• References
  
• MQ-CP
• References
  

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• RIACT
• References
  
• FAM
• References
  
• Modulated RF
• References
  
• RAPT
• References
  
• FASTER
• References
  
• DFS
• References
  

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• MQ-QCPMG-MAS
• References
  
• PFG-MQMAS
• References
  

ST-MAS
衛星躍遷魔角旋轉

1Q-CP MQ-MAS references

Below are provided some NMR references for single-quantum Cross- Polarization followed by MQ-MAS sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling.

• J.-P. Amoureux and M. Pruski,
  Advances in MQMAS NMR, (1)(2)
  in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
  (J. Wiley, Chichester, Vol. 9, 226-251, 2002).
   
• S. E. Ashbrook and S. Wimperis
  Novel two-dimensional NMR methods that combine single-quantum cross-polarization and MQ-MAS of quadrupolar nuclei, (1)(2)
  Chem. Phys. Lett. 2001, 500-508 (2001).
  s.wimperis@exeter.ac.uk
   
• K. H. Lim and C. P. Grey
  ¹⁹F/²³Na multiple quantum cross polarization NMR in solids, (1)(3)
  J. Chem. Phys. 112, 7490-7504 (2000).
   
• S. E. Ashbrook and S. Wimperis
  Multiple-quantum cross-polarization and two-dimensional MQMAS NMR of quadrupolar nuclei, (1)(2)
  J. Magn. Reson. 147, 238-249 (2000).
   
• M. Pruski, C. Fernandez, D. P. Lang, and J.-P. Amoureux
  Measurement of interatomic connectivities in molecular sieves using MQMAS-based methods, (1)(2)
  Catal. Today 49, 401-409 (1999).
   
• F. Taulelle, M. Pruski, J.-P. Amoureux, D. Lang, A. Bailly, C. Huguenard, M. Haouas, C. Gérardin, T. Loiseau, and G. Ferey
  Isomerization of the prenucleation building unit during crystallization of AlPO₄-CJ2: An MQMAS, CP-MQMAS, and HETCOR NMR study, (1)(2)
  J. Am. Chem. Soc. 121, 12148-12153 (1999).
  taulelle@chimie.u-strasbg.fr
   
• C. Fernandez, L. Delevoye, J.-P. Amoureux, D. P. Lang, and M. Pruski
  ²⁷Al{¹H} cross polarization triple-quantum MAS NMR, (1)(3)
  J. Am. Chem. Soc. 119, 6858-6862 (1997).
  christian.fernandez@univ-lille1.fr
   
• M. Pruski, D. P. Lang, C. Fernandez, and J.-P. Amoureux
  MQ MAS NMR with cross-polarization: Spectral editing of high-resolution spectra of quadrupolar nuclei, (1)(2)
  Solid State NMR 7, 327-331 (1997).
   

Related bibliography

• S. E. Ashbrook and S. Wimperis
  Single- and multiple-quantum cross-polarization in NMR of quadrupolar nuclei in static samples, (1)(2)
  Molec. Phys. 98, 1-26 (2000).
  scw@physchem.ox.ac.uk
   
• A. J. Vega
  CP/MAS of quadrupolar S = 3/2 nuclei,
  Solid State NMR 1, 17-32 (1992).