Deuterium-2 NMR




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Isotope Spin Natural
abundance(%)
Quadrupole moment
(10-30m2)
Relative
sensitivity
Absolute
sensitivity
NMR frequency (MHz)
at a field of 2.3488T
Reference
sample
H-1 1/2 99.98 0 1.00 1.00 -100 Me4Si
D-2 1 0.015 0.2860 9.65E-3 1.45E-6 -15.151 (CD3)4Si

Solid-state deuterium NMR references

  1. K. J. Mallikarjunaiah, A. Leftin, J. J. Kinnun, M. J. Justice, A. L. Rogozea, H. I. Petrache, and M. F. Brown
    Solid-state 2H NMR shows equivalence of dehydration and osmotic pressures in lipid membrane deformation,
    Biophys. J. 100, 98-107 (2011).
    Abstract
     
  2. G. Scholz, S. Brehme, R. König, D. Heidemann, and E. Kemnitz
    Crystalline aluminium hydroxide fluorides AlFx(OH)3-x.H2O: Structural insights from 1H and 2H solid state NMR and vibrational spectroscopy,
    J. Phys. Chem. C 114, 10535-10543 (2010).
    Abstract
     
  3. P. D. Frischmann, G. A. Facey, P. Ghi, A. J. Gallant, D. L. Bryce, F. Lelj, and M. J. MacLachlan
    Capsule formation, carboxylate exchange, and DFT exploration of cadmium cluster metallocavitands: highly dynamic supramolecules,
    J. Am. Chem. Soc. 132, 3893-3908 (2010).
    Abstract
     
  4. J. F. Zhu, N. Trefiak, T. Woo, and Y. N. Huang
    An investigation of the adsorption of aromatic hydrocarbons in zeolite Na-Y by solid-state NMR spectroscopy,
    Microporous Mesoporous Mater. 114, 474-484 (2008).
     
  5. G. M. Bowers, D. L. Bish, and R. J. Kirkpatrick
    H2O and cation structure and dynamics in expandable clays: 2H and 39K NMR investigations of hectorite,
    J. Phys. Chem. C 112, 6430-6438 (2008).
     
  6. C. A. Fyfe, R. J. Darton, C. Schneider, and F. Scheffler
    Solid-state NMR investigation of the possible existence of "Nanoblocks" in the clear solution synthesis of MFI materials,
    J. Phys. Chem. C 112, 80-88 (2008).
     
  7. M. Mizuno, Y. Suzuki, K. Endo, M. Murakami, M. Tansho, and T. Shimizu
    Molecular dynamics in paramagnetic materials as studied by magic-angle spinning 2H NMR spectra,
    J. Phys. Chem. A 111, 12954-12960 (2007).
     
  8. E. S. Mananga, R. Roopchand, Y. S. Rumala, and G. S. Boutis
    On the application of magic echo cycles for quadrupolar echo spectroscopy of spin-1 nuclei,
    J. Magn. Reson. 185, 28-37 (2007).
    gboutis@york.cuny.edu
     
  9. C. Odin
    NMR studies of phase transitions,
    Annu. Rep. NMR Spectros. 59, 117-205 (2006).
    christophe.odin@univ-rennes1.fr
     
  10. M. Cutajar, S. E. Ashbrook, and S. Wimperis
    2H double-quantum MAS NMR spectroscopy as a probe of dynamics on the microsecond timescale in solids,
    Chem. Phys. Lett. 423, 276-281 (2006).
    s.wimperis@chem.gle.ac.uk
     
  11. Y. Y. Huang, R. L. Vold, and G. L. Hoatson
    Investigation of multiaxis molecular motion by off-magic angle spinning deuteron NMR,
    J. Chem. Phys. 124, 104504/1-104504/14 (2006).
    rlvold@wm.edu
     
  12. E. S. Mananga, Y. S. Rumala, and G. S. Boutis
    Finite pulse width artifact suppression in spin-1 quadrupolar echo spectra by phase cycling,
    J. Magn. Reson. 181, 296-303 (2006).
    gboutis@york.cuny.edu
     
  13. T. Bräuniger, R. Poupko, Z. Luz, D. Reichert, H. Zimmermann, H. Schmitt, and U. Haeberlen
    Orientational disorder in 1,2,3-trichloro-4,5,6-trimethylbenzene. A single crystal deuterium NMR study of the site populations and dynamics,
    Phys. Chem. Chem. Phys. 3, 1891-1903 (2001).
    Abstract
     
  14. T. Bräuniger, R. Poupko, Z. Luz, H. Zimmermann, and U. Haeberlen
    Quantification of the orientational disorder in ortho-dichlorotetramethylbenzene: A single crystal deuterium nuclear magnetic resonance and x-ray study of the site populations,
    J. Chem. Phys. 115, 8049-8059 (2001).
    Abstract
     
  15. T. Bräuniger, R. Poupko, Z. Luz, P. Gutsche, C. Meinel, H. Zimmermann, and U. Haeberlen
    The dynamic disorder of azulene: A single crystal deuterium nuclear magnetic resonance study,
    J. Chem. Phys. 112, 10858-10870 (2000).
    Abstract
     
  16. A. Detken and H. Zimmermann
    Reorientational tunneling of partially deuterated methyl groups: A single-crystal deuteron NMR study of aspirin-CH2D,
    J. Chem. Phys. 108, 5845-5854 (1998).
    Abstract
     
  17. P. Speier, H. Zimmermann, U. Haeberlen, and Z. Luz
    Dynamic disorder in 2,3-dimethylnaphthalene: a single crystal deuteron nuclear magnetic resonance study,
    Mol. Phys. 95, 1153-1167 (1998).
    Abstract
     
  18. B. Tesche, H. Zimmermann, R. Poupko, and U. Haeberlen
    The single-rotation method of determining quadrupole coupling tensors in monoclinic crystals. Error analysis and application to bullvalene,
    J. Magn. Reson. A 104, 68-77 (1993).
    Abstract
     
  19. H. Eckert, J. P. Yesinowski, and E. M. Stolper
    Quantitative NMR studies of water in silicate glasses,
    Solid State Ionics 32/33, 298-313 (1989).
     
  20. H. Eckert, J. P. Yesinowski, E. M. Stolper, T. R. Stanton, and J. Holloway
    The state of water in rhyolitic glasses: a deuterium NMR study,
    J. Non-Cryst. Solids 93, 93-114 (1987).
     
 

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