Reference for shifted-echo MQ-MAS

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Shifted-echo MQ-MAS references

Below are provided some NMR references about MQ-MAS with shifted-echo pulse sequence applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver-phase relationship.

  1. K. H. Lim, T. Charpentier, and A. Pines
    Efficient triple-quantum excitation in modified RIACT MQMAS NMR for I = 3/2 nuclei, (1)(2)
    J. Magn. Reson. 154, 196-204 (2002).
  2. J.-P. Amoureux and M. Pruski
    Advances in MQMAS NMR, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 226-251, 2002).
  3. L. Frydman
    Fundamentals of MQMAS NMR on half-integer quadrupolar nuclei, (1)(2)
    in Encyclopedia of Nuclear Magnetic Resonance, edited by D. M. Grant and R. K. Harris,
    (J. Wiley, Chichester, Vol. 9, 262-274, 2002).
  4. P. D. Zhao, P. S. Neuhoff, and J. F. Stebbins
    Comparison of FAM mixing to single-pulse mixing in 17O 3Q- and 5Q-MAS NMR of oxygen sites in zeolites, (1)(2)
    Chem. Phys. Lett. 344, 325-332 (2001).
  5. H.-T. Kwak, S. Prasad, Y. Yao, P. J. Grandinetti, J. R. Sachleben, and L. Emsley
    Enhanced sensitivity in RIACT/MQ-MAS NMR experiments using rotor assisted population transfer, (1)(2)
    J. Magn. Reson. 150, 71-80 (2001).
  6. S. Prasad, P. Zhao, J. Huang, J. J. Fitzgerald, and J. S. Shore
    Niobium-93 MQMAS NMR spectroscopy study of alkali and lead niobates, (1)(4)
    Solid State Nucl. Magn. Reson. 19, 45-62 (2001).
  7. T. Vosegaard, D. Massiot, and P. J. Grandinetti
    Sensitivity enhancements in MQ-MAS NMR of spin-5/2 nuclei using modulated RF mixing pulses, (1)(2)(3)
    Chem. Phys. Lett. 326, 454-460 (2000).
  8. T. Charpentier, C. Fermon, and J. Virlet
    Numerical and theoretical analysis of multiquantum MAS experiments, (1)(2)
    J. Chem. Phys. 109, 3116-3130 (1998).
  9. S. P. Brown and S. Wimperis
    Two-dimensional MQ-MAS NMR of quadrupolar nuclei: a comparison of methods, (1)(2)(3)
    J. Magn. Reson. 128, 42-61 (1997).
  10. S. H. Wang, Z. Xu, J. H. Baltisberger, L. M. Bull, J. F. Stebbins, and A. Pines
    MQ MAS and DAS NMR spectroscopy of quadrupolar nuclei, (1)
    Solid State Nucl. Magn. Reson. 8, 1-16 (1997).
  11. J. H. Baltisberger, Z. Xu, J. F. Stebbins, S. H. Wang, and A. Pines
    Triple-quantum 2D 27Al MAS NMR spectroscopy study of aluminosilicate and aluminate crystals and glasses, (1)(2)
    J. Am. Chem. Soc. 118, 7209-7214 (1996).
  12. D. Massiot, B. Touzo, D. Trumeau, J. P. Coutures, J. Virlet, P. Florian, and P. J. Grandinetti
    Two-dimensional MAS isotropic reconstruction sequences for quadrupolar nuclei, (1)(2)(3)
    Solid State Nucl. Magn. Reson. 6, 73-83 (1996).

Related bibliography

  1. P. J. Grandinetti, J. H. Baltisberger, A. Llor, Y. K. Lee, U. Werner, M. A. Eastman, and A. Pines
    Pure-absorption-mode lineshapes and sensitivity in two-dimensional DAS NMR,
    J. Magn. Reson. A 103, 72-81 (1993).

Solid-state NMR bibliography for:

Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91
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