Oxygen-17 NMR references

Isotope	Spin	Natural abundance(%)	Quadrupole moment (10^-30m²)	Relative sensitivity	Absolute sensitivity	NMR frequency (MHz) at a field of 2.3488T	Reference sample
O-17	5/2	0.037	-2.558	2.91E-2	1.08E-5	13.557	D₂O
.	.	.	.	.	.	.	.

Directory of solid-state O-17 NMR references
Polymer, Small Molecule	Crystalline Powder Hydroxide, Micro-Porous, Oxide, Silicate	Amorphous Powder

Solid-state oxygen NMR references

L. Peng, H. Huo, Z. Gan, and C. P. Grey
¹⁷O MQMAS NMR studies of zeolite HY,
Microporous Mesoporous Mater. 109, 156-162 (2008).
A. Soleilhavoup, M. R. Hampson, S. J. Clark, J. S. O. Evans, and P. Hodgkinson
Using ¹⁷O solid-state NMR and first principles calculation to characterise structure and dynamics in inorganic framework materials,
Magn. Reson. Chem. 45, S144-S155 (2008).
A. Wong, I. Hung, A. P. Howes, T. Anupold, J. Past, A. Samoson, S. P. Brown, M. E. Smith, and R. Dupree
The determination of ¹⁷O NMR parameters of hydroxyl oxygen: A combined deuteration and DOR approach,
Magn. Reson. Chem. 45, S68-S72 (2008).
G. Wu, P. Mason, X. Mo, and V. Terskikh
Experimental and computational characterization of the ¹⁷O quadrupole coupling and magnetic shielding NMR tensors for p-nitrobenzaldehyde and formaldehyde,
J. Phys. Chem. A 112, 1024-1032 (2008).
Gang Wu
Solid-state ¹⁷O NMR studies of organic and biological molecules,
Prog. Nucl. Magn. Reson. Spectrosc. 52, 118-169 (2008).
I. Hung, A. Wong, A. P. Howes, T. Anupold, J. Past, A. Samoson, X. Mo, G. Wu, M. E. Smith, S. P. Brown, and R. Dupree
Determination of NMR interaction parameters from double rotation NMR,
J. Magn. Reson. 188, 246-259 (2007).
A. Flambard, L. Montagne, L. Delevoye, and S. Steuernagel
⁹³Nb and ¹⁷O NMR chemical shifts of niobiophosphate compounds,
Solid State NMR 32, 34-43 (2007).
F. H. Larsen, S. Rossano, and I. Farnan
Order and disorder in titanosilicate glass by ¹⁷O MAS, off-MAS, and 3Q-QCPMG-MAS solid-state NMR,
J. Phys. Chem. B 111, 8014-8019 (2007).
S. E. Ashbrook, L. Le-Polles, C. J. Pickard, A. J. Berry, S. Wimperis, and I. Farnan
First-principles calculations of solid-state ¹⁷O and ²⁹Si NMR spectra of Mg₂SiO₄ polymorphs,
Phys. Chem. Chem. Phys. 9, 1587-1598 (2007).
sema@standrews.ac.uk
I. C. M. Kwan, X. Mo, and G. Wu
Probing hydrogen bonding and ion-carbonyl interactions by solid-state ¹⁷O NMR spectroscopy: G-ribbon and G-quartet,
J. Am. Chem. Soc. 129, 2398-2407 (2007).
gangwu@chem.queensu.ca
L. Peng, H. Huo, Y. Liu, and C. P. Grey
¹⁷O magic angle spinning NMR studies of Bronsted acid sites in zeolites HY and HZSM-5,
J. Am. Chem. Soc. 129, 335-346 (2007).
cgrey@notes.cc.sunysb.edu
T. Gullion, K. Yamauchi, M. Okonogi, and T. Asakura
¹³C-¹⁷O REAPDOR NMR as a tool for determining secondary structure in polyamides,
Macromolecules 40, 1363-1365 (2007).
terry.gullion@mail.wvu.edu; asakura@cc.tuat.ac
T. H. Sefzik, J. B. Houseknecht, T. M. Clark, S. Prasad, T. L. Lowary, Z. Gan, and P. J. Grandinetti
Solid-state ¹⁷O NMR in carbohydrates,
Chem. Phys. Lett. 434, 312-315 (2007).
http://www.grandinetti.org/Contact
K. Yamada, H. Honda, T. Yamazaki, M. Yoshida
Solid-state ¹⁷O NMR study of the electric-field-gradient and chemical shielding tensors in polycrystalline gamma-glycine,
Solid State NMR 30, 162-170 (2006).
kyamada@gsc.riken.jp
T. Viefhaus and K. Müller
Solid-state ¹⁷O NMR studies on Yttria-stabilized zirconia,
Int. J. Mat. Res. 97, 508-512 (2006).
k.mueller@ipc.uni-stuttgart.de
T. Viefhaus, T. Bolse, and K. Müller
Oxygen ion dynamics in yttria-stabilized zirconia as evaluated by solid-state ¹⁷O NMR spectroscopy,
Solid State Ionics 177, 3063-3068 (2006).
k.mueller@ipc.uni-stuttgart.de
L. van-Wüllen, N. Sofina, L. Hildebrandt, C. Muhle, and M. Jansen
NMR studies of cation transport in the crystalline ion conductors MCF₃SO₃ (M = Li, Na) and Li₇TaO₆,
Solid State Ionics 177, 1665-1672 (2006).
wullen@uni-muenster.de; m.jansen@fkf.mpg.de
A. Trokiner, A. Yakubovskii, S. Verkhovskii, A. Gerashenko, D. Khomskii
¹⁷O NMR as a conclusive probe of charge-ordering models in half-doped manganites,
Phys. Rev. B 74, 92403/1-92403/4 (2006).
S. K. Lee and J. F. Stebbins
Disorder and the extent of polymerization in calcium silicate and aluminosilicate glasses: ¹⁷O NMR results and quantum chemical molecular orbital calculations,
Geochim. Cosmochim. Acta 70, 4275-4286 (2006).
sungklee@snu.ac.kr
P. Hodgkinson and M. R. Hampson
Quantitative analysis of ¹⁷O exchange and T₁ relaxation data: Application to zirconium tungstate,
Solid State NMR 30, 98-105 (2006).
paul.hodgkinson@durham.ac.uk
S. K. Lee and B. H. Lee
Atomistic origin of germanate anomaly in GeO₂ and Na-germanate glasses: Insights from two-dimensional ¹⁷O NMR and quantum chemical calculations,
J. Phys. Chem. B 110, 16408-16412 (2006).
sungklee@snu.ac.kr
D. Prochnow, A. R. Grimmer, and D. Freude
Solid-state NMR studies of ¹⁷O-enriched pyrophosphates,
Solid State NMR 30, 69-74 (2006).
freude@uni-leipzig.de
A. Brinkmann and A. P. M. Kentgens
Sensitivity enhancement and heteronuclear distance measurements in biological ¹⁷O solid-state NMR,
J. Phys. Chem. B 110, 16089-16101 (2006).
A.Brinkmann@science.ru.nl
A. Flambard, L. Montagne, and L. Delevoye
A new ¹⁷O-isotopic enrichment method for the NMR characterisation of phosphate compounds,
Chem. Commun. 3426-3428 (2006).
lionel.montagne@univ-lille1.fr
S. E. Ashbrook and M. E. Smith
Solid state ¹⁷O NMR - an introduction to the background principles and applications to inorganic materials,
Chem. Soc. Rev. 35, 718-735 (2006).
M.E.Smith.1@warwick.ac.uk
L. S. Du and J. F. Stebbins
Oxygen sites and network coordination in sodium germanate glasses and crystals: High-resolution oxygen-17 and sodium-23 NMR,
J. Phys. Chem. B 110, 12427-12437 (2006).
stebbins@stanford.edu
A. Wong, A. P. Howes, K. J. Pike, V. Lemaître, A. Watts, T. Anupöld, J. Past, A. Samoson, R. Dupree, and M. E. Smith
New limits for solid-state ¹⁷O NMR spectroscopy: Complete resolution of multiple oxygen sites in a simple biomolecule,
J. Am. Chem. Soc. 128, 7744-7745 (2006).
r.dupree@warwick.ac.uk; m.e.smith.1@warwick.ac.uk
S. K. Lee, G. D. Cody, Y. W. Fei, and B. O. Mysen
The effect of Na/Si on the structure of sodium silicate and aluminosilicate glasses quenched from melts at high pressure: A multi-nuclear (Al-27, Na-23, O-17) 1D and 2D solid-state NMR study,
Chem. Geol. 229, 162-172 (2006).
sungklee@snu.ac.kr
B. H. Chen and Y. N. Huang
¹⁷O solid-state NMR spectroscopic studies of the involvement of water vapor in molecular sieve formation by dry-gel conversion,
J. Am. Chem. Soc. 128, 6437-6446 (2006).
yhuang@uwo.ca
J. D. van-Beek, R. Dupree, and M. H. Levitt
Symmetry-based recoupling of ¹⁷O-¹H spin pairs in magic-angle spinning NMR,
J. Magn. Reson. 179, 38-48 (2006).
mhl@soton.ac.uk
A. P. Howes, T. Anupöld, V. Lemaitre, A. Kukol, A. Watts, A. Samoson, M. E. Smith, and R. Dupree
Enhancing resolution and sensitivity of ¹⁷O solid-state NMR through combining double rotation, ¹H decoupling and satellite modulation for biomolecular applications,
Chem. Phys. Lett. 421, 42-46 (2006).
R.Dupree@warwick.ac.uk
S. Prasad, T. M. Clark, R. Sharma, H. T. Kwak, P. J. Grandinetti, and H. Zimmermann
A combined ¹⁷O RAPT and MQ-MAS NMR study of L-leucine,
Solid State NMR 29, 119-124 (2006).
M. R. Hampson, J. S. O. Evans, and P. Hodgkinson
Characterization of oxygen dynamics in ZrW₂O₈,
J. Am. Chem. Soc. 127, 15175-15181 (2005).
john.evans@durham.ac.uk; paul.hodgkinson@durham.ac.uk
E. K. Yildirim and R. Dupree
Study of the relationship between structure and O-17 electric field gradient parameters in some aluminosilicates,
Mod. Phys. Lett. B 19, 1213-1221 (2005).
ek_yildirim@hotmail.com
S. E. Ashbrook and S. Wimperis
Rotor-synchronized acquisition of quadrupolar satellite-transition NMR spectra: practical aspects and double-quantum filtration,
J. Magn. Reson. 177, 44-55 (2005).
s.wimperis@exeter.ac.uk
A. Trokiner, S. Verkhovskii, A. Yakubovskii, K. Kumagai, S. W. Cheong, D. Khomskii, Y. Furukawa, J. S. Ahn, A. Pogudin, V. Ogloblichev, A. Gerashenko, K. Mikhalev, and Yu. Piskunov
Charge-ordered state in half-doped Bi-based manganites studied by ¹⁷O and ²⁰⁹Bi NMR,
Phys. Rev. B 72, 54442/1-54442/9 (2005).
J.-P. Amoureux, A. Flambard, L. Delevoye, and L. Montagne
A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS,
Chem. Commun.3472-3474 (2005).
jean-paul.amoureux@univ-lille1.fr
J.-P. Amoureux, L. Delevoye, G. Fink, F. Taulelle, A. Flambard, and L. Montagne
Implementing SPAM into STMAS: a net sensitivity improvement in high-resolution NMR of quadrupolar nuclei,
J. Magn. Reson. 175, 285-299 (2005).
jean-paul.amoureux@univ-lille1.fr
J. Emery, D. Massiot, P. Lacorre, Y. Laligant, and K. Conder
¹⁷O NMR in room temperature phase of La₂Mo₂O₉ fast oxide ionic conductor,
Magn. Reson. Chem. 43, 366-371 (2005).
joel.emery@univ-lemans.fr
H. Kimura, S. Kanesaka, S. Kuroki, I. Ando, A. Asano, and H. Kurosu
Structural characterization of poly(diethylsiloxane) in the crystalline, liquid crystalline and isotropic phases by solid-state ¹⁷O NMR spectroscopy and ab initio MO calculations,
Magn. Reson. Chem. 43, 209-216 (2005).
skuroki@polymer.titech.ac.jp
M. Zeyer-Dusterer, L. Montagne, G. Palavit, and C. Jager
Combined ¹⁷O NMR and ¹¹B-³¹P double resonance NMR studies of sodium borophosphate glasses,
Solid State NMR 27, 50-64 (2005).
lionel.montagne@univ-lille1.fr; christian.jaeger@bam.de
L. S. Du and J. F. Stebbins
Site connectivities in sodium aluminoborate glasses: multinuclear and multiple quantum NMR results,
Solid State NMR 27, 37-49 (2005).
lsdu@pangea.stanford.edu
L. Peng, Y. Liu, N. Kim, J. E. Readman, and C. P. Grey
Detection of Brønsted acid sites in zeolite HY with high-field ¹⁷O-MAS-NMR techniques,
Nature Mater. 4, 216-219 (2005).
cgrey@notes.cc.sunysb.edu
Jennifer E. Readman, Clare P. Grey, Martine Ziliox, Lucy M. Bull, and Ago Samoson
Comparison of the ¹⁷O NMR spectra of zeolites LTA and LSX,
Solid-State NMR 26, 153-159 (2004).
cgrey@sbchem.sunysb.edu
Burkhard C. Schmidt, Fabrice Gaillard, and Mark E. Smith
Characterisation of ¹⁷O-enriched alumina from a new hydrothermal preparation,
Solid-State NMR 26, 197-202 (2004).
burkhard.schmidt@uni-bayreuth.de
V. Lemaître, M. E. Smith, and A. Watts
A review of oxygen-17 solid-state NMR of organic materials-towards biological applications,
Solid-State NMR 26, 215-235 (2004).
anthony.watts@bioch.ox.ac.uk
K. J. Pike, V. Lemaitre, A. Kukol, T. Anupold, A. Samoson, A. P. Howes, A. Watts, M. E. Smith, and R. Dupree
Solid-state ¹⁷O NMR of amino acids,
J. Phys. Chem. B 108, 9256-9263 (2004).
R.Dupree@warwick.ac.uk; M.E.Smith.1@warwick.ac.uk
D. M. Pickup, F. E. Sowrey, R. J. Newport, P. N. Gunawidjaja, K. O. Drake, and M. E. Smith
The structure of TiO₂-SiO₂ sol-gel glasses from neutron diffraction with isotopic substitution of titanium and ¹⁷O and ⁴⁹Ti solid-state NMR with isotopic enrichment,
J. Phys. Chem. B 108, 10872-10880 (2004).
dmp@kent.ac.uk
M. Zeyer, L. Montagne, and C. Jaeger
Measuring oxygen-phosphorus distances and the orientation of electric field gradient tensors using ¹⁷O-{³¹P} REDOR in phosphate glasses,
Solid State NMR 23, 136-144 (2003).
zeyer@ioq.uni-jena.de; lionel.montagne@univ-lille1.fr
S. Sen and R. E. Youngman
NMR study of Q-speciation and connectivity in K₂O-SiO₂ glasses with high silica content,
J. Non-Cryst. Solids 331, 100-107 (2003).
sens@corning.com
M. D. Glinchuk, A. N. Morozovskaya, A. M. Slipenyuk, and I. P. Bykov
Peculiarities of the radiospectroscopy line shape in nanomaterials,
Appl. Magn. Reson. 24, 333-342 (2003).
glin@materials.kiev.ua
S. K. Lee and J. F. Stebbins
Nature of cation mixing and ordering in Na-Ca silicate glasses and melts,
J. Phys. Chem. B 107, 3141-3148 (2003).
s.lee@gl.ciw.edu
S. K. Lee and J. F. Stebbins
¹⁷O and ²⁷Al MAS and 3QMAS NMR study of synthetic and natural layer silicates,
Chem. Mater. 15, 2605-2613 (2003).
s.lee@gl.ciw.edu
David Rovnyak, Claudiu Filip, Boris Itin, Alan S. Stern, Gerhard Wagner, Robert G. Griffin, and Jeffrey C. Hoch
Multiple-quantum magic-angle spinning spectroscopy using nonlinear sampling,
J. Magn. Reson. 161, 43-55 (2003).
hoch@rowland.org
P. K. Madhu, K. J. Pike, R. Dupree, M. H. Levitt, and M. E. Smith
Modulation-aided signal enhancement in the magic angle spinning NMR of spin-5/2 nuclei,
Chem. Phys. Lett. 367, 150-156 (2003).
mhl@soton.ac.uk; m.e.smith.1@warwick.ac.uk
Flemming H. Larsen and Ian Farnan
²⁹Si and ¹⁷O (Q)CPMG-MAS solid-state NMR experiments as an optimum approach for half-integer nuclei having long T₁ relaxation times,
Chem. Phys. Lett. 357, 403-408 (2002).
ifarnan@esc.cam.ac.uk
D. L. Bryce, K. Eichele, and R. E. Wasylishen
An ¹⁷O NMR and quantum chemical study of monoclinic and orthorhombic polymorphs of triphenylphosphine oxide,
Inorg. Chem. 42, 5085-5096 (2003).
roderick.wasylishen@ualberta.ca
R. E. Wasylishen and D. L. Bryce
A revised experimental absolute magnetic shielding scale for oxygen,
J. Chem. Phys. 117, 10061-10066 (2002).
roderick.wasylishen@ualberta.ca
C. J. Fontenot, J. W. Wiench, G. L. Schrader, and M. Pruski
¹⁷O MAS and 3QMAS NMR investigation of crystalline V₂O₅ and layered V₂O₅ nH₂O gels,
J. Am. Chem. Soc. 124, 8435-8444 (2002).
mpruski@iastate.edu
G. Wu, S. Dong, R. Ida, and N. Reen
A solid-state ¹⁷O nuclear magnetic resonance study of nucleic acid bases,
J. Am. Chem. Soc. 124, 1768-1777 (2002).
gangwu@chem.queensu.ca
P. S. Neuhoff, P. Shao, and J. F. Stebbins
Effect of extraframework species on ¹⁷O NMR chemical shifts in zeolite A,
Microporous Mesoporous Mater. 55, 239-251 (2002).
stebbins@pangea.stanford.edu
Namjun Kim and Clare P. Grey
Probing oxygen motion in disordered anionic conductors with ¹⁷O and ⁵¹V MAS NMR spectroscopy,
Science 297, 1317-1320 (2002).
S. E. Ashbrook, S. Antonijevic, A. J. Berry, and S. Wimperis
Motional broadening: an important distinction between multiple-quantum and satellite-transition MAS NMR of quadrupolar nuclei,
Chem. Phys. Lett. 364, 634-642 (2002).
s.wimperis@exeter.ac.uk
S. E. Ashbrook, A. J. Berry, and S. Wimperis
¹⁷O multiple-quantum MAS NMR study of pyroxenes,
J. Phys. Chem. B 106, 773-778 (2002).
s.wimperis@exeter.ac.uk

Related bibliography

Raisa I. Maksimovskaya and Gennady M. Maksimov
⁹⁵Mo and ¹⁷O NMR studies of aqueous molybdate solutions,
Inorg. Chem. 46, 3688-3695 (2007).
rimax@catalysis.nsk.su

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