Sodium-23 NMR references

Isotope	Spin	Natural abundance(%)	Quadrupole moment (10^-30m²)	Relative sensitivity	Absolute sensitivity	NMR frequency (MHz) at a field of 2.3488T	Reference sample
Na-23	3/2	100	10.4	9.25E-2	9.25E-2	-26.451	NaCl
.	.	.	.	.	.	.	.

Directory of solid-state Na-23 NMR references
Single Crystal	Crystalline Powder Micro-Porous, Na2HPO4 NaH2PO4, Na2SO4, Na2SO3, NaCl, NaNO3, NaNO2...	Amorphous Powder

Solid-state sodium NMR references

Mattias Edén
Homonuclear dipolar recoupling of half-integer spin quadrupolar nuclei: Techniques and applications,
Solid State Nucl. Magn. Reson. 36, 1-10 (2009).
Abstract
Zhen Wu and Shangwu Ding
Prevention of spinning induced sample deterioration during long time solid state NMR experiments of quadrupolar spin systems,
Solid State Nucl. Magn. Reson. 35, 214-216 (2009).
Abstract
Sharon E. Ashbrook and Stephen Wimperis
Spin-locking of half-integer quadrupolar nuclei in nuclear magnetic resonance of solids: Second-order quadrupolar and resonance offset effects,
J. Chem. Phys. 131, 194509/1-194509/15 (2009).
Abstract
M. Nausner, J. Brus, M. Häubl, N. Müller, and W. Schoefberger
Characterization of the sodium binding sites in microcrystalline ATP by ²³Na-solid-state NMR and ab initio calculations,
Inorg. Chim. Acta 362, 1071-1077 (2009).
Abstract
Renée Siegel, João Rocha, and Luís Mafra
Combining STMAS and CRAMPS NMR spectroscopy: High-resolution HETCOR NMR spectra of quadrupolar and ¹H nuclei in solids,
Chem. Phys. Lett. 470, 337-341 (2009).
Abstract
Mattias Edén
Determination of absolute quadrupolar tensor orientations by double-quantum NMR on powders,
Chem. Phys. Lett. 470, 318-324 (2009).
Abstract
J. F. Zhu, N. Trefiak, T. Woo, and Y. N. Huang
An investigation of the adsorption of aromatic hydrocarbons in zeolite Na-Y by solid-state NMR spectroscopy,
Microporous Mesoporous Mater. 114, 474-484 (2008).
L. Gueudre, A. A. Quoineaud, G. Pirngruber, and P. Leflaive
Evidence of multiple cation site occupation in zeolite NaY with high Si/Al ratio,
J. Phys. Chem. C 112, 10899-10908 (2008).
E. S. Mananga, C. D. Hsu, S. Ishmael, T. Islam, and G. S. Boutis
Probing the validity of average Hamiltonian theory for spin I = 1, 3/2 and 5/2 nuclei by analyzing a simple two-pulse sequence,
J. Magn. Reson. 193, 10-22 (2008).
C. Tien, E. V. Charnaya, M. K. Lee, S. V. Baryshnikov, D. Michel, W. Bohlmann
NMR studies of structure and ferroelectricity for Rochelle salt nanoparticles embedded in mesoporous sieves,
J. Phys.: Condens. Matter 20, 215205/1-215205/6 (2008).
M. Inukai and K. Takeda
Studies on multiple-quantum magic-angle-spinning NMR of half-integer quadrupolar nuclei under strong rf pulses with a microcoil,
Concepts Magn. Reson. B 33, 115-123 (2008).
B. Hu, J. P. Amoureux, J. Trebosc, and S. Hafner
Through-space MP-CPMAS experiments between spin-1/2 and half-integer quadrupolar nuclei in solid-state NMR,
J. Magn. Reson. 192, 8-16 (2008).
M. J. Thrippleton, T. J. Ball, and S. Wimperis
Satellite transitions acquired in real time by magic angle spinning (STARTMAS): "Ultrafast" high-resolution MAS NMR spectroscopy of spin I = 3/2 nuclei ,
J. Chem. Phys. 128, 34507/1-34507/9 (2008).
T. Gullion
Dipolar recoupling of I = 1/2, S = 3/2 spin pairs with SEDOR for static and spinning samples,
Magn. Reson. Chem. 45, S65-S67 (2008).
M. Xu and K. D. M. Harris
Triple-quantum ²³Na MAS NMR spectroscopy as a technique for probing polymorphism in sodium salts,
Cryst. Growth Des. 8, 6-10 (2008).
W. Stroiek, C. M. Felise, H. Eckert, B. Ewald, and R. Kniep
Site discrimination in the crystalline borophosphate Na₅B₂P₃O₁₃ using advanced solid-state NMR techniques,
Solid State NMR 32, 89-98 (2007).
C. M. Widdifield, J. A. Tang, C. L. B. Macdonald, and R. W. Schurko
Investigation of structure and dynamics in the sodium metallocenes CpNa and CpNa·THF via solid-state NMR, X-ray diffraction and computational modelling,
Magn. Res. Chem. 45, S116-S128 (2007).
Vladimir K. Michaelis, Pedro M. Aguiar, and Scott Kroeker
Probing alkali coordination environments in alkali borate glasses by multinuclear magnetic resonance,
J. Non-Cryst. Solids 353, 2582-2590 (2007).
J. F. Zhu, N. Mosey, T. Woo, and Y. N. Huang
Study of the adsorption of toluene in zeolite LiNa-Y by solid-state NMR Spectroscopy,
J. Phys. Chem. C 111, 13427-13436 (2007).
M. T. Rinke, L. Zhang, and H. Eckert
Structural integration of tellurium oxide into mixed-network-former glasses: connectivity distribution in the system NaPO₃-TeO₂,
ChemPhysChem. 8, 1988-1998 (2007).
J. Trebosc, B. Hu, J. P. Amoureux, and Z. Gan
Through-space R³-HETCOR experiments between spin-1/2 and half-integer quadrupolar nuclei in solid-state NMR,
J. Magn. Reson. 186, 220-227 (2007).
jean-paul.amoureux@univ-lillel.fr
G. Mali
Spin-locking and recoupling of homonuclear dipolar interaction between spin-3/2 nuclei under magic-angle sample spinning,
J. Magn. Reson. 185, 318-325 (2007).
gregor.mali@ki.si
F. Angeli, M. Gaillard, P. Jollivet, and T. Charpentier
Contribution of ⁴³Ca MAS NMR for probing the structural configuration of calcium in glass,
Chem. Phys. Lett. 440, 324-328 (2007).
frederic.angeli@cea.fr
J. Trebosc, J.-P. Amoureux, and Z. H. Gan
Comparison of high-resolution solid-state NMR MQMAS and STMAS methods for half-integer quadrupolar nuclei,
Solid State NMR 31, 1-9 (2007).
jean-paul.amoureux@univ-lille1.fr
P. Florian, E. M. Anghel, and C. Bessada
Structural description of the Na₂B₄O₇-Na₃AlF₆-TiO₂ system. 2. A multinuclear NMR approach of melts and solids,
J. Phys. Chem. B 111, 968-978 (2007).
bessada@cnrs-orleans.fr
M. Alecci, S. Romanzetti, J. Kaffanke, A. Celik, H. P. Wegener, and N. J. Shah
Practical design of a 4 Tesla double-tuned RF surface coil for interleaved ¹H and ²³Na MRI of rat brain,
J. Magn. Reson. 181, 203-211 (2006).
Abstract
M. Eden, D. Zhou, and J. H. Yu
Improved double-quantum NMR correlation spectroscopy of dipolar-coupled quadrupolar spins,
Chem. Phys. Lett. 431, 397-403 (2006).
mattias@physc.su.se
C. Martineau, M. Body, C. Legein, G. Silly, J. Y. Buzaré, and F. Fayon
Multinuclear high-resolution NMR study of compounds from the ternary system NaF-CaF₂-AlF₃: From determination to modeling of NMR parameters,
Inorg. Chem. 45, 10215-10223 (2006).
charlotte.martineau.etu@univ-lemans.fr
D. L. Bryce, S. Adiga, E. K. Elliott, and G. W. Gokel
Solid-state ²³Na NMR study of sodium lariat ether receptors exhibiting cation-π interactions,
J. Phys. Chem. A 110, 13568-13577 (2006).
S. E. Ashbrook, L. Le-Polles, R. Gautier, C. J. Pickard, and R. I. Walton
²³Na multiple-quantum MAS NMR of the perovskites NaNbO₃ and NaTaO₃,
Phys. Chem. Chem. Phys. 8, 3423-3431 (2006).
sema@st-andrews.ac.uk
M. Itoh, I. Yamauchi, T. Kozuka, T. Suzuki, T. Yamauchi, J. Yamaura, and Y. Ueda
Charge disproportionation and metal-insulator transition in the quasi-one-dimensional conductor βNa_0.33V₂O₅: ²³Na NMR study of a single crystal,
Phys. Rev. B 74, 54434/1-54434/14 (2006).
X. Y. Wen, X. J. Ai, J. X. Dong, J. Yang, C. H. Ye, and F. Deng
Reaction of layered sodium disilicate SKS-6 with calcium chloride solution as revealed by solid state NMR spectroscopy: Exploring the calcium ion extracting mechanism of SKS-6,
Solid State NMR 30, 89-97 (2006).
dengf@wipm.ac.cn
S. P. Puls and H. Eckert
Site discrimination in mixed-alkali glasses studied by cross-polarization NMR,
J. Phys. Chem. B 110, 14253-14261 (2006).
eckerth@uni-muenster.de
F. Muñoz, L. Montagne, L. Delevoye, A. Duran, L. Pascual, S. Cristol, and J. F. Paul
Phosphate speciation in sodium borosilicate glasses studied by nuclear magnetic resonance,
J. Non-Cryst. Solids 352, 2958-2968 (2006).
lionel.montagne@univ-lille1.fr
C. C. de-Araujo, W. Strojek, L. Zhang, H. Eckert, G. Poirier, S. J. L. Ribeiro, and Y. Messaddeq
Structural studies of NaPO₃-WO₃ glasses by solid state NMR and Raman spectroscopy,
J. Mater. Chem. 16, 3277-3284 (2006).
eckerth@uni-muenster.de
X. Xu and R. J. Kirkpatrick
NaCl interaction with interfacially polymerized polyamide films of reverse osmosis membranes: A solid-state ²³Na NMR study,
J. Membrane Sci. 280, 226-233 (2006).
xiangxu1@illinoisalumni.org; kirkpat@uiuc.edu
R. Kharrazian and P. M. Jakob
Dynamics of ²³Na during completely balanced steady-state free precession,
J. Magn. Reson. 179, 73-84 (2006).
rakharra@physik.uni-wuerzburg.de
M. Edén
Quadrupolar coupling selective cross-polarization in solid state NMR,
Phys. Chem. Chem. Phys. 8, 1994-1999 (2006).
mattias@physc.su.se
A. Y. H. Lo, R. W. Schurko, M. Vettraino, B. O. Skadtchenko, M. Trudeau, and D. M. Antonelli
Solid-state ²³Na and ⁷Li NMR investigations of sodium- and lithium-reduced mesoporous titanium oxides,
Inorg. Chem. 45, 1828-1838 (2006).
rschurko@uwindsor.ca; danton@uwindsor.ca
M. Nyman, A. J. Celestian, J. B. Parise, G. P. Holland, and T. M. Alam
Solid-state structural characterization of a rigid framework of lacunary heteropolyniobates,
Inorg. Chem. 45, 1043-1052 (2006).
mdnyman@sandia.gov
M. Kotecha, S. Chaudhuri, C. P. Grey, and L. Frydman
Dynamic effects in MAS and MQMAS NMR spectra of half-integer quadrupolar nuclei: Calculations and an application to the double perovskite cryolite,
J. Am. Chem. Soc. 127, 16701-16712 (2005).
lucio.frydman@weizmann.ac.il
C. H. Liao, P. C. Chang, H. M. Kao, and K. H. Lii
Synthesis, crystal structure, and solid-state NMR spectroscopy of a salt-inclusion stannosilicate: [Na₃F][SnSi₃O₉],
Inorg. Chem. 44, 9335-9339 (2005).
hmkao@cc.ncu.edu.tw; liikh@cc.ncu.edu.tw
R. Kumar, W. Ling, W. Schoefberger, and A. Jerschow
Separated quadrupolar field experiment,
J. Magn. Reson. 172, 209-213 (2005).
alexej.jerschow@nyu.edu
J. D. Epping, W. Strojek, and H. Eckert
Cation environments and spatial distribution in Na₂O-B₂O₃ glasses: New results from solid state NMR,
Phys. Chem. Chem. Phys. 7, 2384-2389 (2005).
H. Trill, H. Eckert, and V. I. Srdanov
NMR study of interacting F centers in Na₈[Al₆Si₆O₂₄]Cl₂ sodalite,
Phys. Rev. B 71, 014412/1-014412/6 (2005).
J. P. Amoureux, L. Delevoye, S. Steuernagel, Z. Gan, S. Ganapathy, and L. Montagne
Increasing the sensitivity of 2D high-resolution NMR methods applied to quadrupolar nuclei,
J. Magn. Reson. 172, 268-278 (2005).
jean-paul.amoureux@univ-lille1.fr
C. Johnson, E. A. Moore, and M. Mortimer
Periodic ab initio calculation of nuclear quadrupole parameters as an assignment tool in solid-state NMR spectroscopy: applications to ²³Na NMR spectra of crystalline materials,
Solid State NMR 27, 155-164 (2005).
m.mortimer@open.ac.uk
G. Silly, C. Legein, J. Y. Buzaré, and F. Calvayrac
Electric field gradients in fluoride crystalline powders: correlation of NMR measurements with ab initio calculations,
Solid State NMR 25, 241-251 (2004).
gilles.silly@univ-lemans.fr
R. Siegel, T. T. Nakashima, and R. E. Wasylishen
Signal enhancement of NMR spectra of half-integer quadrupolar nuclei in solids using hyperbolic secant pulses,
Chem. Phys. Lett. 388, 441-445 (2004).
roderick.wasylishen@ualberta.ca
R. W. Schurko, M. J. Willans, B. Skadtchenko, and D. M. Antonelli
Solid-state ²³Na and ¹³C NMR characterization of Na₃C₆₀,
J. Solid State Chem. 177, 2255-2264 (2004).
rschurko@uwindsor.ca
G. Mali and V. Kaucic
Enhancing sensitivity or resolution of homonuclear correlation experiment for half-integer quadrupolar nuclei,
J. Magn. Reson. 171, 48-56 (2004).
gregor.mali@ki.si
A. Wong, R. D. Whitehead, Z. H. Gan, and G. Wu
A solid-state NMR and computational study of sodium and potassium tetraphenylborates: ²³Na and ³⁹K NMR signatures for systems containing cation-pi interactions,
J. Phys. Chem. A 108, 10551-10559 (2004).
gangwu@chem.queensu.ca
T. G. Ajithkumar, E. R. H. van-Eck, and A. P. M. Kentgens
Homonuclear correlation experiments for quadrupolar nuclei, spinning away from the magic angle,
Solid State NMR 26, 180-186 (2004).
arno.kentgens@nmr.kun.nl
A. Goldbourt, E. Vinogradov, G. Goobes, and S. Vega
High resolution heteronuclear correlation NMR spectroscopy between quadrupolar nuclei and protons in the solid state,
J. Magn. Reson. 169, 342-350 (2004).
shimon.vega@weizmann.ac.il
Z. H. Gan and H. T. Kwak
Enhancing MQMAS sensitivity using signals from multiple coherence transfer pathways,
J. Magn. Reson. 168, 346-351 (2004).
gan@magnet.fsu.edu
H. X. Yang, R. I. Walton, S. Antonijevic, S. Wimperis, and A. C. Hannon
Local order of amorphous zeolite precursors from ²⁹Si[¹H] CPMAS and ²⁷Al and ²³Na MQMAS NMR and evidence for the nature of medium-range order from neutron diffraction,
J. Phys. Chem. B 108, 8208-8217 (2004).
r.i.walton@exeter.ac.uk
G. Mali and F. Taulelle
Detecting proximities between quadrupolar nuclei by double-quantum NMR,
Chem. Commun. 868-869 (2004).
gregor.mali@ki.si
S. E. Ashbrook and S. Wimperis
Spin-locking of half-integer quadrupolar nuclei in nuclear magnetic resonance of solids: Creation and evolution of coherences,
J. Chem. Phys. 120, 2719-2731 (2004).
s.wimperis@exeter.ac.uk
T. Bräuniger, K. Ramaswamy, and P. K. Madhu
Enhancement of the central-transition signal in static and magic-angle-spinning NMR of quadrupolar nuclei by frequency-swept fast amplitude-modulated pulses,
Chem. Phys. Lett. 383, 403-410 (2004).
braeuniger@physik.uni-halle.de; madhu@tifr.res.in
Z. H. Liu, F. Deng, and S. W. Ding
Effects of pulse strength, width, and sample spinning speed on the spectral spin diffusion of multiquantum coherences of spin-3/2 quadrupolar nuclei,
J. Chem. Phys. 120, 740-748 (2004).
dengf@wipm.ac.cn; ding@mail.nsysu.edu.tw
A. Wong, G. Wu
Selective binding of monovalent cations to the stacking G-quartet structure formed by guanosine 5'-monophosphate: A solid-state NMR study,
J. Am. Chem. Soc. 125, 13895-13905 (2003).
gangwu@chem.queensu.ca
M. Edén and L. Frydman
Homonuclear NMR correlations between half-integer quadrupolar nuclei undergoing magic-angle spinning,
J. Phys. Chem. B 107, 14598-14611 (2003).
Lucio.Frydman@weizinann.ac.il
A. D. Bain
Exact calculation, using angular momentum, of combined Zeeman and quadrupolar interactions in NMR,
Molec. Phys. 101, 3163-3175 (2003).
bain@mcmaster.ca
C. M. Morais, M. Lopes, C. Fernandez, and J. Rocha
Assessing the potential of fast amplitude modulation pulses for improving triple-quantum magic angle spinning NMR spectra of half-integer quadrupolar nuclei,
Magn. Reson. Chem. 41, 679-688 (2003).
rocha@dq.ua.pt
X. J. Ai, L. Chen, J. X. Dong, C. H. Ye, and F. Deng
Variation of sodium coordination during the hydration processes of layered sodium disilicates as studied by ²³Na MQMAS and ¹H <-> ²³Na CP/MAS NMR spectroscopy,
J. Mater. Chem. 13, 614-621 (2003).
dengf@wipm.ac.cn
M. J. Willans and R. W. Schurko
A solid-state NMR and ab initio study of sodium metallocenes,
J. Phys. Chem. B 107, 5144-5161 (2003).
rschurko@uwindsor.ca

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Solid-state sodium NMR references

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Sodium-23 NMR
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