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> Nitrogen
| Isotope | Spin | Natural abundance(%) |
Quadrupole moment (10-30m2) |
Relative sensitivity |
Absolute sensitivity |
NMR frequency (MHz) at a field of 2.3488T |
Reference sample |
|---|---|---|---|---|---|---|---|
| N-14 | 1 | 99.63 | 2.044 | 1.01E-3 | 1.01E-3 | -7.224 | CH3NO2 |
| N-15 | 1/2 | 0.37 | 0 | 1.04E-3 | 3.85E-6 | 10.133 | MeNO2 |
Solid-state nitrogen NMR references
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N. M. Trease and P. J. Grandinetti
Solid-state nuclear magnetic resonance in the rotating tilted frame,
J. Chem. Phys. 128, 52318/1-52318/12 (2008).
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S. Cavadini, A. Abraham, and G. Bodenhausen
Coherence transfer between spy nuclei and nitrogen-14 in solids,
J. Magn. Reson. 190, 160-164 (2008).
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C. A. Fyfe, R. J. Darton, C. Schneider, and F. Scheffler
Solid-state NMR investigation of the possible existence of "Nanoblocks" in the clear solution synthesis of MFI materials,
J. Phys. Chem. C 112, 80-88 (2008).
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S. Cavadini, S. Antonijevic, A. Lupulescu, and G. Bodenhausen
Indirect detection of nitrogen-14 in solid-state NMR spectroscopy,
ChemPhysChem. 8, 1363-1374 (2007).
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T. N. Rudakov
Some aspects of spin-locking effect in nitrogen-14 quadrupolar spin-system,
Chem. Phys. Lett. 443, 269-273 (2007).
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H. J. Jakobsen, A. R. Hove, H. Bildsoe, J. Skibsted, M. Brorson
Long-term stability of rotor-controlled MAS frequencies to 0.1 Hz proved by 14N MAS NMR experiments and simulations,
J. Magn. Reson. 185, 159-163 (2007).
hja@chem.au.dk
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Z. H. Gan, J.-P. Amoureux, and J. Trebosc
Proton-detected 14N MAS NMR using homonuclear decoupled rotary resonance,
Chem. Phys. Lett. 435, 163-169 (2007).
gan@magnet.fsu.edu
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Z. H. Gan
13C/14N heteronuclear multiple-quantum correlation with rotary resonance and REDOR dipolar recoupling,
J. Magn. Reson. 184, 39-43 (2007).
gan@magnet.fsu.edu
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Z. H. Gan
Measuring multiple carbon-nitrogen distances in natural abundant solids using R-RESPDOR NMR,
Chem. Commun.4712-4714 (2006).
gan@magnet.fsu.edu
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A. R. Hove, H. Bildsoe, J. Skibsted, M. Brorson, and H. J. Jakobsen
Probing crystal structures and transformation reactions of ammonium molybdates by 14N MAS NMR spectroscopy,
Inorg. Chem. 45, 10873-10881 (2006).
hja@chem.au.dk
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H. J. Jakobsen, A. R. Hove, R. G. Hazell, H. Bildsøe, and J. Skibsted
Solid-state 14N MAS NMR of ammonium ions as a spy to structural insights for ammonium salts,
Magn. Reson. Chem. 44, 348-356 (2006).
hja@chem.au.dk
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J. P. Yesinowski
69,71Ga and 14N high-field NMR of gallium nitride films,
phys. stat. sol. (c) 2, 2399-2402 (2005).
yesinows@ccs.nrl.navy.mil
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A. P. Purdy, J. P. Yesinowski, and A. T. Hanbicki
Synthesis, solid-state NMR, and magnetic characterization of h-GaN containing magnetic ions,
phys. stat. sol. (c) 2, 2437-2440 (2005).
purdy1@ccs.nrl.navy.mil
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E. A. Hill and J. P. Yesinowski
A slow turning method for measuring large anisotropic interactions in inhomogeneously broadened NMR spectra,
J. Chem. Phys. 106, 8650-8659 (1997).
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E. A. Hill and J. P. Yesinowski
Solid-state 14N NMR techniques for studying slow molecular motions,
J. Chem. Phys. 107, 346-354 (1997).
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E. A. Hill and J. P. Yesinowski
Wide-line 14N NMR in solids and reorientation-induced redistribution of isochromats,
J. Am. Chem. Soc. 118, 6798-6799 (1996).
Related bibliography
-
S. Cavadini, S. Antonijevic, A. Lupulescu, and G. Bodenhausen
Indirect detection of nitrogen-14 in solids via protons by nuclear magnetic resonance spectroscopy,
J. Magn. Reson. 182, 168-172 (2006).
Sasa.Antonijevic@epfl.ch
Solid-state NMR bibliography for
- Aluminum-27 (鋁)
- Antimony-121/123 (銻)
- Arsenic-75 (砷)
- Barium-135/137 (鋇)
- Beryllium-9 (鈹)
- Bismuth-209 (鉍)
- Boron-11 (硼)
- Bromine-79/81 (溴)
- Calcium-43 (鈣)
- Cesium-133 (銫)
- Chlorine-35/37 (氯)
- Chromium-53 (鉻)
- Cobalt-59 (鈷)
- Copper-63/65 (銅)
- Deuterium-2 (氘)
- Gallium-69/71 (鎵)
- Germanium-73 (鍺)
- Gold-197 (金)
- Hafnium-177/179 (鉿)
- Indium-113-115 (銦)
- Iodine-127 (碘)
- Iridium-191/193 (銥)
- Krypton-83 (氪)
- Lanthanum-139 (鑭)
- Lithium-6/7 (鋰)
- Magnesium-25 (鎂)
- Manganese-55 (錳)
- Mercury-201 (銾)
- Molybdenum-95/97 (鉬)
- Neon-21 (氖)
- Nickel-61 (鎳)
- Niobium-93 (鈮)
- Nitrogen-14 (氮)
- Osmium-189 (鋨)
- Oxygen-17 (氧)
- Palladium-105 (鈀)
- Potassium-39/41 (鉀)
- Rhenium-185/187 (錸)
- Rubidium-85/87 (銣)
- Ruthenium-99/101 (釕)
- Scandium-45 (鈧)
- Sodium-23 (鈉)
- Strontium-87 (鍶)
- Sulfur-33 (硫)
- Tantalum-181 (鉭)
- Titanium-47/49 (鈦)
- Vanadium-51 (釩)
- Xenon-131 (氥)
- Zinc-67 (鋅)
- Zirconium-91 (鋯)
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