Nutation NMR pulse programs




Home and Applets > Pulse Program

Some nutation NMR pulse programs for half-integer quadrupole spins are provided for Bruker spectrometers.

SF = BF1 + SR (Larmor frequency of reference sample)

SFO1 = BF1 + O1 (spectrometer frequency)


*** Outline ***


AVANCE III spectrometers
with topSpin2.1 operating system

amplitude-modulated
experiments:

  • Z-filter
    The same pulse program as that defined for XWINNMR 3.5 operating system
  • SPAM-echo/antiecho (2D only)
    The only change is the addtion of 3u delay before the two signal storage lines in the pulse program for XWINNMR 3.5 operating system
  • MQMAS data processing:
    Shearing the 2D spectrum with AU program xfshear

phase-modulated
experiments:

  • Multiplex SPAM (2D only)
    The same pulse program as that defined for XWINNMR 3.5 operating system
  • The AU program MSM (Multiplex SPAM MQ) remains valid


1-dimensional experiments:

  • qcpmg.fau, pulse program for performing CPMG experiment via SGU in channel 1, which samples continuously.
  • qcpmgadd.jt from Julien Trébosc, AU program to store echos from qcpmg.fau experiment by adding them up. Use absolute scale for Y-axis to check the amplitude of echo in the FID window.
    If digmod is used, convert data to analog with convdta command.
    ALWAYS use this AU program on a COPY of dataset.
  • qcpmg-split, AU program for splitting CPMG echo train acquired with qcpmg.fau pulse program. These echoes allow T2 measurement.
    ALWAYS use this AU program on a COPY of dataset.
  • hpdeccpmg.fau, pulse program for performing high power decoupling experiment with CPMG detection via SGU in channel 1, which samples continuously
  • cpcpmg.fau, pulse program for performing basic cross-polarisation experiment with CPMG detection via SGU in channel 1, which samples continuously


Bruker Biospin manuals (PDF file)

Other manuals (PDF file)

AU programs

Jython

The C++ Resources Network > Reference > C Library > cstdio(stdio.h)

Installing and setting up Topspin (PDF file)

AVANCE spectrometers
with xwinnmr 3.5 operating system

These pulse programs are available for both 1D and 2D NMR experiments.

amplitude-modulated
experiments:

phase-modulated
experiments:


1-dimensional experiments:

  • qcpmgall.av, pulse program which samples continuously, including ALL pulses and ringdown delays
  • au_qcpmg, AU program which takes out data points sampled during pulses and ring down delays.
    If digmod is used, convert data to analog with convdta command.
    ALWAYS use this AU program on a COPY of dataset.
  • qcpmgaddjt from Julien Trébosc, AU program which stores echos from qcpmgall.av pulse program by adding them up.
    Use absolute scale for Y-axis to check the amplitude of echo in the FID window.
    If digmod is used, convert data to analog with convdta command.
    ALWAYS use this AU program on a COPY of dataset.
  • qcpmgsplit, AU program for splitting CPMG echo train acquired with qcpmgall.av pulse program. These echoes allow T2 measurement.
  • hpdecqcpmgall.av, pulse program for performing CPMG experiment with high power decoupling , which samples continuously, including ALL pulses and ringdown delays
  • cpqcpmgall.av, pulse program for performing basic cross-polarisation experiment with CPMG detection, which samples continuously, including ALL pulses and ringdown delays


AVANCE hardware

Acquisition commands and parameters

Processing commands and parameters

Au programming

Z-filtered STMAS pulse program

One pulse program with digital phase for the receiver

Ecole Polytechnique Fédérale de Lausanne: Experimental aspects of NMR (PDF file)

Bruker NMR guide, version 3.5

ENS Lyon - Pulse Programs Library

Iowa State University - Mei Hong research group

AVANCE AQX spectrometers
with xwinnmr 2.6 operating system

1-dimensional experiments:


MSL and ASX spectrometers

1-dimensional experiments:

2-dimensional experiments:


TopSpin file folder tree

topspin file folder tree


TopSpin BSMS

topspin BSMS

Enter bsmsdisp on the command line

[Contact me] - Last updated January 30, 2010
Copyright © 2002- pascal-man.com. All rights reserved.