Titanium-47 and titanium-49 NMR references

Isotope	Spin	Natural abundance(%)	Quadrupole moment (10^-30m²)	Relative sensitivity	Absolute sensitivity	NMR frequency (MHz) at a field of 2.3488T	Reference sample
Ti-47	5/2	7.28	30.2	2.09E-3	1.52E-4	-5.637	TiCl₄
Ti-49	7/2	5.51	24.7	3.76E-3	2.07E-4	-5.638

Solid-state titanium NMR references

A. J. Rossini, I. Hung, and Robert W. Schurko
Solid-state ^47/49Ti NMR of titanocene chlorides,
J. Phys. Chem. Lett. 1, 2989-2998 (2010).
Abstract
G. W. Wagner and B. Itin
Comment on "²⁷Al, ⁴⁷Ti,⁴⁹Ti, ³¹P, and ¹³C MAS NMR study of VX, GD, and HD reactions with nanosize Al₂O₃, conventional Al₂O₃ and TiO₂, and aluminum and titanium metal",
J. Phys. Chem. C 112, 9962-9962 (2008).
G. W. Wagner, L. R. Procell, and S. Munavalli
²⁷Al, ⁴⁷Ti, ⁴⁹Ti, ³¹P, and ¹³C MAS NMR study of VX, GD, and HD reactions with nanosize Al₂O₃, conventional Al₂O₃ and TiO₂, and aluminum and titanium metal,
J. Phys. Chem. C 111, 17564-17569 (2007).
F. H. Larsen, I. Farnan, and A. S. Lipton
Separation of ⁴⁷Ti and ⁴⁹Ti solid-state NMR lineshapes by static QCPMG experiments at multiple fields,
J. Magn. Reson. 178, 228-236 (2006).
fhl@kvl.dk
Boštjan Zalar, Andrija Lebar, Janez Seliger, Robert Blinc, Valentin V. Laguta, and Mitsuru Itoh
NMR study of disorder in BaTiO₃ and SrTiO₃,
Phys. Rev. B 71, 64107/1-64107/12 (2005).
Thomas Bräuniger, P. K. Madhu, André Pampel, and Detlef Reichert
Application of fast amplitude-modulated pulse trains for signal enhancement in static and magic-angle-spinning ^47,49Ti-NMR spectra,
Solid-State NMR 26, 114-120 (2004).
braeuniger@physik.uni-halle.de
Christel Gervais, Delphine Veautier, Mark E. Smith, Florence Babonneau, Philippe Belleville, and Clément Sanchez
Solid state ^47,49Ti, ⁸⁷Sr and ¹³⁷Ba NMR characterisation of mixed barium/strontium titanate perovskites,
Solid-State NMR 26, 147-152 (2004).
gervais@ccr.jussieu.fr
D. M. Pickup, F. E. Sowrey, R. J. Newport, P. N. Gunawidjaja, K. O. Drake, and M. E. Smith
The structure of TiO₂-SiO₂ sol-gel glasses from neutron diffraction with isotopic substitution of titanium and ¹⁷O and ⁴⁹Ti solid-state NMR with isotopic enrichment,
J. Phys. Chem. B 108, 10872-10880 (2004).
dmp@kent.ac.uk
T. J. Bastow and G. W. West
Defects and hyperfine interactions in Ni-Y intermetallics (Y = Al, Ga, In, Ti) via ²⁷Al, ⁴⁷Ti, ⁶¹Ni, ^69,67Ga and ¹¹⁵In nuclear resonance,
J. Phys.: Condens. Matter 15, 8389-8406 (2003).
T. Kiyama, S. Fujisawa, H. Saitoh, M. Itoh, K. Kodama, and M. Takigawa
NMR study of orbital ordering in RTiO3 (R = Y, Gd, and La),
Physica B 329, 733-735 (2003).
kiyama@nucc.cc.nagoya-u.ac.jp
T. Kiyama and M. Itoh
Presence of 3d quadrupole moment in LaTiO₃ studied by ^47,49Ti NMR,
Phys. Rev. Lett. 91, 167202/1-167202/4 (2003).
S. Ganapathy, K. U. Gore, R. Kumar, and J.-P. Amoureux
Multinuclear (²⁷Al, ²⁹Si, ^47,49Ti) solid-state NMR of titanium substituted zeolite USY,
Solid State NMR 24, 184-195 (2003).
ganapathy@ems.ncl.res.in
B. Zalar, V. V. Laguta, and R. Blinc
NMR evidence for the coexistence of order-disorder and displacive components in barium titanate,
Phys. Rev. Lett. 90, 37601/1-37601/4 (2003).
D. Padro, V. Jennings, M. E. Smith, R. Hoppe, P. A. Thomas, and R. Dupree
Variations of titanium interactions in solid state NMR-correlations to local structure,
J. Phys. Chem. B 106, 13176-13185 (2002).
m.e.smith.1@warwick.ac.uk; r.dupree@warwick.ac.uk
D. Padro, A. P. Howes, M. E. Smith, and R. Dupree
Determination of titanium NMR parameters of ATiO₃ compounds: correlations with structure distorsion,
Solid State NMR 15, 231-236 (2000).
L. V. Dmitrieva, L. S. Vorotilova, I. S. Podkorytov, and M. E. Shelyapina
A comparison of NMR spectral parameters of ⁴⁷Ti and ⁴⁹Ti nuclei in rutile and anatase,
Phys. Solid State 41, 1097-1099 (1999).
T. J. Bastow and H. J. Whitfield
^47,49Ti NMR: evolution of crystalline TiO₂ from the gel state,
Chem. Mater. 11, 3518-3520 (1999).
T. J. Bastow, M. A. Gibson, and C. T. Forwood
^47,49Ti NMR: hyperfine interactions in oxides and metals,
Solid State NMR 12, 201-209 (1998).
A. Labouriau and W. L. Earl
Titanium solid-state NMR in anatase, brookite and rutile,
Chem. Phys. Lett. 270, 278-284 (1997).

Related bibliography

Andrea Labouriau, Kevin C. Ott, Jon Rau, and William L. Earl
Titanium-substituted zeolites and molecular sieves investigated by NMR,
J. Phys. Chem. B 104, 5890-5896 (2000).
R. Koch and T. Bruhn
Theoretical ⁴⁹Ti NMR chemical shifts,
J. Mol. Model 12, 723-729 (2006).
rainer.koch@uni-oldenburg.de
José C. Vites and Mary M. Lynam
Titanium 1993,
Coord. Chem. Rev. 146, 1-15 (1995).

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Solid-state titanium NMR references

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More solid-state Ti-47/49 NMR references.

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Titanium-47 and titanium-49 NMR
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