NMR pulse sequence:
CP-MAS

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CP-MAS

Some NMR references about CP-MAS pulse sequences applied to half-integer quadrupole spins:

  1. S. P. Puls and H. Eckert
    Site discrimination in mixed-alkali glasses studied by cross-polarization NMR,
    J. Phys. Chem. B 110, 14253-14261 (2006).
  2. M. Edén
    Quadrupolar coupling selective cross-polarization in solid state NMR,
    Phys. Chem. Chem. Phys. 8, 1994-1999 (2006).
  3. Gregor Mali and Venceslav Kaucic
    Determination of distances between aluminum and spin-1/2 nuclei using cross polarization with very weak radio-frequency fields,
    J. Chem. Phys. 117, 3327-3339 (2002).
  4. G. Mali, A. Meden, A. Ristic, N. N. Tusar, and V. Kaucic
    Interaction of dipropylamine template molecules with the framework of as-synthesized AlPO4-31,
    J. Phys. Chem. B 106, 63-69 (2002).
  5. J.-P. Amoureux and M. Pruski
    Theoretical and experimental assessment of single- and multiple-quantum cross-polarization in solid state NMR,
    Mol. Phys. 100, 1595-1613 (2002).
  6. S. E. Ashbrook and S. Wimperis
    Single- and multiple-quantum cross-polarization in NMR of quadrupolar nuclei in static samples,
    Mol. Phys. 98, 1-26 (2000).
  7. J. M. Egan, R. M. Wenslow, and K. T. Mueller
    Mapping aluminum/phosphorus connectivities in aluminophosphate glasses,
    J. Non-Cryst. Solids 261, 115-126 (2000).
  8. M. A. Eastman
    Examples of Hartmann-Hahn match conditions for CP/MAS between two half-integer quadrupolar nuclei,
    J. Magn. Reson. 139, 98-108 (1999).
  9. S. Ding and C. A. McDowell
    Application of Floquet theory to quadrupolar nuclear spin-5/2 nuclei in solids undergoing sample rotation,
    Mol. Phys. 95, 841-848 (1998).
  10. M. Tomaselli, D. deGraw, J. L. Yarger, M. P. Augustine, and A. Pines
    Scalar and anisotropic J interactions in undoped InP: a triple-resonance NMR study,
    Phys. Rev. B 58, 8627-8633 (1998).
  11. Jerry C. C. Chan, Marko Bertmer, and Hellmut Eckert
    Double-quantum cross-polarization between half-integer quadrupolar spin systems: 11B <-> 23Na and 11B <-> 27Al,
    Chem. Phys. Lett. 292, 154-160 (1998).
  12. E. R. H. van Eck and M. E. Smith
    Orientation of the quadrupole and dipole tensors of hydroxyl groups by 17O quadrupole separated local field NMR,
    J. Chem. Phys. 108, 5904-5912 (1998).
  13. S. M. De Paul, M. Ernst, J. S. Shore, J. F. Stebbins, and A. Pines
    Cross-polarization from quadrupolar nuclei to silicon using low-radio-frequency amplitudes during MAS,
    J. Phys. Chem. B 101, 3240-3249 (1997).
  14. L. van Wüllen, L. Züchner, W. Müller-Warmuth, and H. Eckert
    11B{27Al} and 27Al{11B} double resonance experiments on a glassy sodium aluminoborate,
    Solid State Nucl. Magn. Reson. 6, 203-212 (1996).
  15. G. G. Almond, R. K. Harris, and K. R. Franklin
    1H, 29Si and 1H, 23Na heteronuclear shift correlation in octosilicate via cross-polarisation,
    Solid State Nucl. Magn. Reson. 6, 31-38 (1996).
  16. T. P. Jarvie, R. M. Wenslow, and K. T. Mueller
    High-resolution solid-state heteronuclear correlation NMR for quadrupolar and spin-1/2 nuclei,
    J. Am. Chem. Soc. 117, 570-571 (1995).
  17. S. Ding and C. A. McDowell
    Theoretical calculations of the CPMAS spectral lineshapes of half-integer quadrupole systems,
    J. Magn. Reson. A 114, 80-87 (1995).
  18. P. J. Barrie
    Distorted powder lineshapes in 27Al CP/MAS NMR spectroscopy of solids,
    Chem. Phys. Lett. 208, 486-490 (1993).
  19. S. Hayashi and K. Hayamizu
    Errata: Line shapes in CP/MAS NMR spectra of half-integer quadrupolar nuclei,
    Chem. Phys. Lett. 205, 597-597 (1993).
  20. S. Hayashi and K. Hayamizu
    Line shapes in CP/MAS NMR spectra of half-integer quadrupolar nuclei,
    Chem. Phys. Lett. 203, 319-324 (1993).
  21. C. A. Fyfe, K. T. Mueller, H. Grondey, and K. C. Wong-Moon
    Solid-state double-resonance NMR experiments involving quadrupolar and spin 1/2 nuclei,
    J. Phys. Chem. 97, 13484-13495 (1993).
  22. C. A. Fyfe, H. Grondey, K. T. Mueller, K. C. Wong-Moon, and T. Markus
    Coherence transfer involving quadrupolar nuclei in solids: 27Al<->31P cross-polarization NMR in the molecular sieves VPI-5,
    J. Am. Chem. Soc. 114, 5876-5878 (1992).
  23. A. J. Vega
    CP/MAS of quadrupolar S = 3/2 nuclei,
    Solid State Nucl. Magn. Reson. 1, 17-32 (1992).
  24. R. K. Harris and G. J. Nesbitt
    Cross polarization for quadrupolar nuclei---Proton to sodium-23,
    J. Magn. Reson. 78, 245-256 (1988).

Related bibliography

  1. M. Ernst-M, H. Geen, and B. H. Meier
    Amplitude-modulated decoupling in rotating solids: A bimodal Floquet approach,
    Solid State Nucl. Magn. Reson. 29, 2-21 (2006).
  2. K. Gopalakrishnan and G. Bodenhausen
    Cross polarization from spins I = 1/2 to spins S = 1 in nuclear magnetic resonance with magic angle sample spinning,
    J. Chem. Phys. 124, 194311/1-194311/14 (2006).
  3. S. V. Dvinskikh and V. I. Chizhik
    Cross-polarization with radio-frequency field phase and amplitude modulation under magic-angle spinning conditions,
    J. Exp. Theo. Phys. 102, 91-101 (2006).
  4. C. Lejeune, C. Coelho, L. Bonhomme-Coury, T. Azaïs, J. Maquet, and C. Bonhomme
    Studies of silicophosphate derivatives by 31P -> 29Si CP MAS NMR,
    Solid State Nucl. Magn. Reson. 27, 242-246 (2005).
  5. Robert E. Taylor
    13C CP/MAS: Application to glycine,
    Concepts Magn. Reson. A 22, 79-89 (2004).
  6. Robert E. Taylor
    Setting up 13C CP/MAS experiments,
    Concepts Magn. Reson. A 22, 37-49 (2004).
  7. H. Kampermann, A. D. Bain, and R. S. Dumont
    Residual dipolar coupling in the CP/MAS nuclear magnetic resonance spectra of spin-1/2 nuclei coupled to quadrupolar nuclei application of floquet theory,
    J. Chem. Phys. 116, 2464-2471 (2002).
  8. G. Metz, X. Wu, and S. O. Smith
    Ramped-amplitude cross polarization in magic-angle-spinning NMR,
    J. Magn. Reson. A 110, 219-227 (1994).
  9. B. H. Meier
    Cross polarization under fast magic angle spinning: thermodynamical considerations,
    Chem. Phys. Lett. 188, 201-207 (1992).
  10. E. O. Stejskal and J. Schaefer
    Removal of artifacts from cross-polarization NMR experiments,
    J. Magn. Reson. 18, 560-563 (1975).
  11. A. Pines, M. G. Gibby, and J. S. Waugh
    Proton-enhanced NMR of dilute spins in solids,
    J. Chem. Phys. 59, 569-590 (1973).
  12. S. R. Hartmann and E. L. Hahn
    Nuclear double resonance in the rotating frame,
    Phys. Rev. 128, 2042-2053 (1962).

Solid-state NMR bibliography for:

Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91
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