NMR pulse sequence:
CP-MAS




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CP-MAS

Some NMR references about CP-MAS pulse sequences applied to half-integer quadrupole spins:

  • S. P. Puls and H. Eckert
    Site discrimination in mixed-alkali glasses studied by cross-polarization NMR,
    J. Phys. Chem. B 110, 14253-14261 (2006).
    eckerth@uni-muenster.de
     
  • M. Edén
    Quadrupolar coupling selective cross-polarization in solid state NMR,
    Phys. Chem. Chem. Phys. 8, 1994-1999 (2006).
    mattias@physc.su.se
     
  • Gregor Mali and Venceslav Kaucic
    Determination of distances between aluminum and spin-1/2 nuclei using cross polarization with very weak radio-frequency fields,
    J. Chem. Phys. 117, 3327-3339 (2002).
     
  • G. Mali, A. Meden, A. Ristic, N. N. Tusar, and V. Kaucic
    Interaction of dipropylamine template molecules with the framework of as-synthesized AlPO4-31,
    J. Phys. Chem. B 106, 63-69 (2002).
     
  • J.-P. Amoureux and M. Pruski
    Theoretical and experimental assessment of single- and multiple-quantum cross-polarization in solid state NMR,
    Molec. Phys. 100, 1595-1613 (2002).
    mpruski@iastate.edu
     
  • S. E. Ashbrook and S. Wimperis
    Single- and multiple-quantum cross-polarization in NMR of quadrupolar nuclei in static samples,
    Mol. Phys. 98, 1-26 (2000).
    scw@physchem.ox.ac.uk
     
  • J. M. Egan, R. M. Wenslow, and K. T. Mueller
    Mapping aluminum/phosphorus connectivities in aluminophosphate glasses,
    J. Non-Cryst. Solids 261, 115-126 (2000).
    ktm2@psu.edu
     
  • M. A. Eastman
    Examples of Hartmann-Hahn match conditions for CP/MAS between two half-integer quadrupolar nuclei,
    J. Magn. Reson. 139, 98-108 (1999).
     
  • S. Ding and C. A. McDowell
    Application of Floquet theory to quadrupolar nuclear spin-5/2 nuclei in solids undergoing sample rotation,
    Mol. Phys. 95, 841-848 (1998).
     
  • M. Tomaselli, D. deGraw, J. L. Yarger, M. P. Augustine, and A. Pines
    Scalar and anisotropic J interactions in undoped InP: a triple-resonance NMR study,
    Phys. Rev. B 58, 8627-8633 (1998).
     
  • Jerry C. C. Chan, Marko Bertmer, and Hellmut Eckert
    Double-quantum cross-polarization between half-integer quadrupolar spin systems: 11B <-> 23Na and 11B <-> 27Al,
    Chem. Phys. Lett. 292, 154-160 (1998).
    eckerth@uni-muenster.de
     
  • E. R. H. van Eck and M. E. Smith
    Orientation of the quadrupole and dipole tensors of hydroxyl groups by 17O quadrupole separated local field NMR,
    J. Chem. Phys. 108, 5904-5912 (1998).
    erhv@ukc.ac.uk
     
  • S. M. De Paul, M. Ernst, J. S. Shore, J. F. Stebbins, and A. Pines
    Cross-polarization from quadrupolar nuclei to silicon using low-radio-frequency amplitudes during MAS,
    J. Phys. Chem. B 101, 3240-3249 (1997).
     
  • L. van Wüllen, L. Züchner, W. Müller-Warmuth, and H. Eckert
    11B{27Al} and 27Al{11B} double resonance experiments on a glassy sodium aluminoborate,
    Solid State NMR 6, 203-212 (1996).
     
  • G. G. Almond, R. K. Harris, and K. R. Franklin
    1H, 29Si and 1H, 23Na heteronuclear shift correlation in octosilicate via cross-polarisation,
    Solid State NMR 6, 31-38 (1996).
     
  • T. P. Jarvie, R. M. Wenslow, and K. T. Mueller
    High-resolution solid-state heteronuclear correlation NMR for quadrupolar and spin-1/2 nuclei,
    J. Am. Chem. Soc. 117, 570-571 (1995).
     
  • S. Ding and C. A. McDowell
    Theoretical calculations of the CPMAS spectral lineshapes of half-integer quadrupole systems,
    J. Magn. Reson. A 114, 80-87 (1995).
     
  • P. J. Barrie
    Distorted powder lineshapes in 27Al CP/MAS NMR spectroscopy of solids,
    Chem. Phys. Lett. 208, 486-490 (1993).
     
  • S. Hayashi and K. Hayamizu
    Errata: Line shapes in CP/MAS NMR spectra of half-integer quadrupolar nuclei,
    Chem. Phys. Lett. 205, 597-597 (1993).
     
  • S. Hayashi and K. Hayamizu
    Line shapes in CP/MAS NMR spectra of half-integer quadrupolar nuclei,
    Chem. Phys. Lett. 203, 319-324 (1993).
     
  • C. A. Fyfe, K. T. Mueller, H. Grondey, and K. C. Wong-Moon
    Solid-state double-resonance NMR experiments involving quadrupolar and spin 1/2 nuclei,
    J. Phys. Chem. 97, 13484-13495 (1993).
     
  • C. A. Fyfe, H. Grondey, K. T. Mueller, K. C. Wong-Moon, and T. Markus
    Coherence transfer involving quadrupolar nuclei in solids: 27Al<->31P cross-polarization NMR in the molecular sieves VPI-5,
    J. Am. Chem. Soc. 114, 5876-5878 (1992).
     
  • A. J. Vega
    CP/MAS of quadrupolar S = 3/2 nuclei,
    Solid State NMR 1, 17-32 (1992).
     
  • R. K. Harris and G. J. Nesbitt
    Cross polarization for quadrupolar nuclei---Proton to sodium-23,
    J. Magn. Reson. 78, 245-256 (1988).
     

Related bibliography

  • M. Ernst-M, H. Geen, and B. H. Meier
    Amplitude-modulated decoupling in rotating solids: A bimodal Floquet approach,
    Solid State NMR 29, 2-21 (2006).
    maer@ethz.ch
     
  • K. Gopalakrishnan and G. Bodenhausen
    Cross polarization from spins I = 1/2 to spins S = 1 in nuclear magnetic resonance with magic angle sample spinning,
    J. Chem. Phys. 124, 194311/1-194311/14 (2006).
    geoffrey.bodenhausen@epfl.ch
     
  • S. V. Dvinskikh and V. I. Chizhik
    Cross-polarization with radio-frequency field phase and amplitude modulation under magic-angle spinning conditions,
    J. Exp. Theo. Phys. 102, 91-101 (2006).
    sergey@physc.su.se
     
  • C. Lejeune, C. Coelho, L. Bonhomme-Coury, T. Azaïs, J. Maquet, and C. Bonhomme
    Studies of silicophosphate derivatives by 31P -> 29Si CP MAS NMR,
    Solid State NMR 27, 242-246 (2005).
    bonhomme@ccr.jussieu.fr
     
  • Robert E. Taylor
    13C CP/MAS: Application to glycine,
    Concepts Magn. Reson. A 22, 79-89 (2004).
    taylor@chem.ucla.edu
     
  • Robert E. Taylor
    Setting up 13C CP/MAS experiments,
    Concepts Magn. Reson. A 22, 37-49 (2004).
    taylor@chem.ucla.edu
     
  • H. Kampermann, A. D. Bain, and R. S. Dumont
    Residual dipolar coupling in the CP/MAS nuclear magnetic resonance spectra of spin-1/2 nuclei coupled to quadrupolar nuclei application of floquet theory,
    J. Chem. Phys. 116, 2464-2471 (2002).
    bain@mcmaster.ca
     
  • G. Metz, X. Wu, and S. O. Smith
    Ramped-amplitude cross polarization in magic-angle-spinning NMR,
    J. Magn. Reson. A 110, 219-227 (1994).
     
  • B. H. Meier
    Cross polarization under fast magic angle spinning: thermodynamical considerations,
    Chem. Phys. Lett. 188, 201-207 (1992).
     
  • E. O. Stejskal and J. Schaefer
    Removal of artifacts from cross-polarization NMR experiments,
    J. Magn. Reson. 18, 560-563 (1975).
     
  • A. Pines, M. G. Gibby, and J. S. Waugh
    Proton-enhanced NMR of dilute spins in solids,
    J. Chem. Phys. 59, 569-590 (1973).
     
  • S. R. Hartmann and E. L. Hahn
    Nuclear double resonance in the rotating frame,
    Phys. Rev. 128, 2042-2053 (1962).
     
 
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