NMR pulse sequence:
ST-MAS NMR
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Satellite Transition Magic Angle Spinning references

Below are provided some NMR references about ST-MAS applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver-phase relationship.

  1. Takafumi Takahashi, Shunsuke Kashiwakura, Koji Kanehashi, and Tetsuya Nagasaka
    First high-resolution 11B nuclear magnetic resonance (NMR) spectra of coal fly ash by satellite-transition magic angle spinning (STMAS) NMR, (1)(2)
    Energy Fuels 23, 1778-1780 (2009).
    Abstract
  2. Takafumi Takahashi, Koji Kanehashi, Yuichi Shimoikeda, Takahiro Nemoto, and Koji Saito
    Practical comparison of sensitivity and resolution between STMAS and MQMAS for 27Al, (1)(2)(3)
    J. Magn. Reson. 198, 228-235 (2009).
    Abstract
  3. J. Trebosc, J.-P. Amoureux, and Z. H. Gan
    Comparison of high-resolution solid-state NMR MQMAS and STMAS methods for half-integer quadrupolar nuclei, (1)
    Solid State Nucl. Magn. Reson. 31, 1-9 (2007).
  4. J.-P. Amoureux and J. Trébosc
    Homogeneous broadenings in 2D solid-state NMR of half-integer quadrupolar nuclei, (1)(2)
    J. Magn. Reson. 179, 311-316 (2006).
  5. O. B. Lapina, D. F. Khabibulin, K. V. Romanenko, Z. H. Gan, M. G. Zuev, V. N. Krasil'nikov, and V. E. Fedorov
    93Nb NMR chemical shift scale for niobia systems,
    Solid State Nucl. Magn. Reson. 28, 204-224 (2005).
  6. J.-P. Amoureux, A. Flambard, L. Delevoye, and L. Montagne
    A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS, (1)(2)
    Chem. Commun.3472-3474 (2005).
  7. J.-P. Amoureux, L. Delevoye, G. Fink, F. Taulelle, A. Flambard, and L. Montagne
    Implementing SPAM into STMAS: a net sensitivity improvement in high-resolution NMR of quadrupolar nuclei, (1)(2)(3)
    J. Magn. Reson. 175, 285-299 (2005).
  8. Sharon E. Ashbrook and Stephen Wimperis,
    High-resolution NMR of quadrupolar nuclei in solids: the satellite-transition magic angle spinning (STMAS) experiment, (1)(2)(3)
    Progr. Nucl. Magn. Reson. Spectrosc. 45, 53-108 (2004).
  9. N. G. Dowell, S. E. Ashbrook, and S. Wimperis
    Satellite-transition MAS NMR of low-gamma nuclei at natural abundance: sensitivity, practical implementation, and application to 39K (I = 3/2) and 25Mg (I = 5/2), (1)(2)
    J. Phys. Chem. B 108, 13292-13299 (2004).
  10. Z. Gan, P. Srinivasan, J. R. Quine, S. Steuernagel, and B. Knott
    Third-order effect in solid-state NMR of quadrupolar nuclei,
    Chem. Phys. Lett. 367, 163-169 (2003).
  11. J.-P. Amoureux, C. Morais, J. Trebosc, J. Rocha, and C. Fernandez
    I-STMAS, a new high-resolution solid-state NMR method for half-integer, (1)(2)(3)
    Solid State Nucl. Magn. Reson. 23, 213-223 (2003).
  12. S. Wi, S. E. Ashbrook, S. Wimperis, L. Frydman
    Second-order quadrupole-shielding effects in magic-angle spinning solid-state nuclear magnetic resonance,
    J. Chem. Phys. 118, 3131-3140 (2003).
  13. H. T. Kwak and Z. H. Gan
    Double-quantum filtered STMAS, (1)(2)(3)
    J. Magn. Reson. 164, 369-372 (2003).
  14. S. E. Ashbrook and S. Wimperis
    SCAM-STMAS: satellite-transition MAS NMR of quadrupolar nuclei with self-compensation for magic-angle misset, (1)(2)(3)
    J. Magn. Reson. 162, 402-416 (2003).
  15. J.-P. Amoureux, C. Huguenard, F. Engelke, and F. Taulelle
    Unified representation of MQMAS and STMAS NMR of half-integer quadrupolar nuclei,
    Chem. Phys. Lett. 356, 497-504 (2002).
  16. S. E. Ashbrook and S. Wimperis
    Satellite-transition MAS NMR of spin I = 3/2, 5/2, 7/2, and 9/2 nuclei: sensitivity, resolution, and practical implementation, (1)(2)(3)
    J. Magn. Reson. 156, 269-281 (2002).
  17. C. Huguenard, F. Taulelle, B. Knott, and Z. Gan
    Optimizing STMAS, (1)(2)(3)
    J. Magn. Reson. 156, 131-137 (2002).
  18. S. E. Ashbrook and S. Wimperis
    High-resolution NMR spectroscopy of quadrupolar nuclei in solids: satellite-transition MAS with self-compensation for magic-angle misset, (1)(2)(3)
    J. Am. Chem. Soc. 124, 11602-11603 (2002).
  19. Z. Gan, P. Gor'kov, T. A. Cross, A. Samoson, and D. Massiot
    Seeking higher resolution and sensitivity for NMR of quadrupolar nuclei at ultrahigh magnetic fields,
    J. Am. Chem. Soc. 124, 5634-5635 (2002).
  20. K. J. Pike, S. E. Ashbrook, and S. Wimperis
    Two-dimensional satellite-transition MAS NMR of quadrupolar nuclei: shifted echoes, high-spin nuclei and resolution, (1)(2)(3)
    Chem. Phys. Lett. 345, 400-408 (2001).
  21. Z. Gan
    Satellite transition magic-angle spinning nuclear magnetic resonance of half-integer quadrupolar nuclei, (1)(2)(3)
    J. Chem. Phys. 114, 10845-10853 (2001).
  22. Z. Gan
    Isotopic NMR spectra of half-integer quadrupolar nuclei using satellite transitions and magic-angle spinning, (3)
    J. Am. Chem. Soc. 122, 3242-3243 (2000).

Solid-state NMR bibliography for:

Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91
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