Boron-11 NMR references

Isotope	Spin	Natural abundance(%)	Quadrupole moment (10^-30m²)	Relative sensitivity	Absolute sensitivity	NMR frequency (MHz) at a field of 2.3488T	Reference sample
B-10	3	19.58	8.459	1.99E-2	3.90E-3	-10.746	BF₃ Et₂O
B-11	3/2	80.42	4.059	0.17	0.13	-32.084

Directory of solid-state B-11 NMR references
Crystalline Powder	Amorphous Powder

Solid-state boron NMR references

J. P. Amoureux, J. Trebosc, and G. Tricot
Measurement of through-space connectivities between spin-1/2 and quadrupolar nuclei in solid-state NMR: the TEDOR-MQMAS method,
Magn. Reson. Chem. 45, S187-S191 (2008).
W. Stroiek, C. M. Felise, H. Eckert, B. Ewald, and R. Kniep
Site discrimination in the crystalline borophosphate Na₅B₂P₃O₁₃ using advanced solid-state NMR techniques,
Solid State NMR 32, 89-98 (2007).
G. Guella, B. Patton, and A. Miotello
Kinetic features of the platinum catalyzed hydrolysis of sodium borohydride from ¹¹B NMR measurements,
J. Phys. Chem. C 111, 18744-18750 (2007).
Y. H. Sehlleier, A. Verhoeven, and M. Jansen
NMR studies of short and intermediate range ordering of amorphous Si-B-N-C-H pre-ceramic at the pyrolysis stage of 600 °C,
J. Mater. Chem. 17, 4316-4319 (2007).
Vladimir K. Michaelis, Pedro M. Aguiar, and Scott Kroeker
Probing alkali coordination environments in alkali borate glasses by multinuclear magnetic resonance,
J. Non-Cryst. Solids 353, 2582-2590 (2007).
D. Zielniok, C. Cramer, and H. Eckert
Structure/property correlations in ion-conducting mixed-network former glasses: Solid-state NMR studies of the system Na₂O-B₂O₃-P₂O₅,
Chem. Mater. 19, 3162-3170 (2007).
S. Indris, P. Heitjans, J. Hattendorf, W.-D. Zeitz, and T. Bredow
Local electronic structure in MgB₂from ¹²B β-NMR,
Phys. Rev. B 75, 024502/1-024502/6 (2007).
T. Emmler, O. Tsetsgee, G. Buntkowsky, M. Weinmann, F. Aldinger, and K. Muller
¹¹B{¹⁵N} redor and ¹¹B spin echo studies for structural characterization of Si-B-C-N precursor ceramics,
Soft Mater. 4, 207-225 (2007).
k.mueller@ipc.uni-stuttgart.de
L. van-Wullen, S. Wegner, and G. Tricot
Structural changes above the glass transition and crystallization in aluminophosphate glasses: An in situ high-temperature MAS NMR study,
J. Phys. Chem. B 111, 7529-7534 (2007).
A. C. Stowe, W. J. Shaw, J. C. Linehan, B. Schmid, and T. Autrey
In situ solid state ¹¹B MAS-NMR studies of the thermal decomposition of ammonia borane: mechanistic studies of the hydrogen release pathways from a solid state hydrogen storage material,
Phys. Chem. Chem. Phys. 9, 1831-1836 (2007).
D. Caurant, O. Majerus, E. Fadel, M. Lenoir, C. Gervais, and O. Pinet
Effect of molybdenum on the structure and on the crystallization of SiO₂-Na₂O-CaO-B₂O₃ glasses,
J. Am. Ceram. Soc. 90, 774-783 (2007).
daniel-caurant@enscp.fr
P. Florian, E. M. Anghel, and C. Bessada
Structural description of the Na₂B₄O₇-Na₃AlF₆-TiO₂ system. 2. A multinuclear NMR approach of melts and solids,
J. Phys. Chem. B 111, 968-978 (2007).
bessada@cnrs-orleans.fr
Z. Szalay and J. Rohonczy
A multinuclear NMR study of sodium-borovanadophosphate glasses,
J. Non-Cryst. Solids 353, 295-301 (2007).
rohonczy@chem.elte.hu
D. S. Mao and G. H. Lu
The effect of B₂O₃ addition on the crystallization of amorphous TiO₂-ZrO₂ mixed oxide,
Solid State Chem. 180, 484-488 (2007).
dsmao1106@yahoo.com.cn
G. Guella, C. Zanchetta, B. Patton, and A. Miotello
New insights on the mechanism of palladium-catalyzed hydrolysis of sodium borohydride from ¹¹B NMR measurements,
J. Phys. Chem. B 110, 17024-17033 (2006).
guella@science.unitn.it
S. I. Lee, K. Saito, K. Kanehashi, M. Hatakeyama, S. Mitani, S. H. Yoon, Y. Korai, and I. Mochida
¹¹B NMR study of the BF₄^- anion in activated carbons at various stages of charge of EDLCs in organic electrolyte,
Carbon 44, 2578-2586 (2006).
mochida@asem.kyushu-u.ac.jp
I. Eswaramoorthi and A. K. Dalai
Synthesis, characterisation and catalytic performance of boron substituted SBA-15 molecular sieves,
Microporous Mesoporous Mater. 93, 1-11 (2006).
ajay.dalai@usask.ca
F. Muñoz, L. Montagne, L. Delevoye, A. Duran, L. Pascual, S. Cristol, and J. F. Paul
Phosphate speciation in sodium borosilicate glasses studied by nuclear magnetic resonance,
J. Non-Cryst. Solids 352, 2958-2968 (2006).
lionel.montagne@univ-lille1.fr
S. Prasad, T. M. Clark, T. H. Sefzik, H. T. Kwak, Z. H. Gan, and P. J. Grandinetti
Solid-state multinuclear magnetic resonance investigation of Pyrex,
J. Non-Cryst. Solids 352, 2834-2840 (2006).
http://www.grandinetti.org/Contact
T. I. Koranyi and J. B. Nagy
Distribution of aluminum and boron in the periodical building units of boron-containing beta zeolites,
J. Phys. Chem. B 110, 14728-14735 (2006).
koranyi@chemres.hu
M. Jansen, J. C. Schön, and L. van-Wüllen
The route to the structure determination of amorphous solids: A case study of the ceramic Si₃B₃N₇,
Angew. Chem. Int. Ed. 45, 4244-4263 (2006).
m.jansen@fkf.mpg.de
S. E. Ashbrook, N. G. Dowell, I. Prokes, and S. Wimperis
Nuclear overhauser effect (NOE) enhancement of ¹¹B NMR spectra of borane adducts in the solid state,
J. Am. Chem. Soc. 128, 6782-6783 (2006).
s.wimperis@chem.gla.ac.uk
Y. Kim and R. J. Kirkpatrick
¹¹B NMR investigation of boron interaction with mineral surfaces: Results for boehmite, silica gel and illite,
Geochim. Cosmochim. Acta 70, 3231-3238 (2006).
ygkim@knu.ac.kr
Y. N. Huang, Z. M. Yan, and R. Richer
Characterization of BAPO- and SAPO-based mesoporous materials by solid-state NMR spectroscopy,
Chem. Mater. 17, 6545-6554 (2005).
yhuang@uwo.ca
J. Yang, A. M. Zheng, M. J. Zhang, Q. Luo, Y. Yue, C. H. Ye, X. Lu, and F. Deng
Bronsted and Lewis acidity of the BF₃/gamma-Al₂O₃ alkylation catalyst as revealed by solid-state NMR spectroscopy and DFT quantum chemical calculations,
J. Phys. Chem. B 109, 13124-13131 (2005).
dengf@wipm.ac.cn
J. D. Epping, H. Eckert, A. W. Imre, and H. Mehrer
Structural manifestations of the mixed-alkali effect: NMR studies of sodium rubidium borate glasses,
J. Non-Cryst. Solids 351, 3521-3529 (2005).
eckerth@uni-muenster.de
J. D. Epping, W. Strojek, and H. Eckert
Cation environments and spatial distribution in Na₂O-B₂O₃ glasses: New results from solid state NMR,
Phys. Chem. Chem. Phys. 7, 2384-2389 (2005).
S. Elbers, W. Strojek, L. Koudelka, and H. Eckert
Site connectivities in silver borophosphate glasses: new results from ¹¹B{³¹P} and ³¹P{¹¹B} rotational echo double resonance NMR spectroscopy,
Solid State NMR 27, 65-76 (2005).
eckerth@uni-muenster.de
M. Zeyer-Dusterer, L. Montagne, G. Palavit, and C. Jager
Combined ¹⁷O NMR and ¹¹B-³¹P double resonance NMR studies of sodium borophosphate glasses,
Solid State NMR 27, 50-64 (2005).
lionel.montagne@univ-lille1.fr; christian.jaeger@bam.de
L. S. Du and J. F. Stebbins
Site connectivities in sodium aluminoborate glasses: multinuclear and multiple quantum NMR results,
Solid State NMR 27, 37-49 (2005).
lsdu@pangea.stanford.edu
P. M. Aguiar and S. Kroeker
Medium-range order in cesium borate glasses probed by double-resonance NMR,
Solid State NMR 27, 10-15 (2005).
scott_kroeker@umanitoba.ca
S. J. Hwang, C. Y. Chen, and S. I. Zones
Boron sites in borosilicate zeolites at various stages of hydration studied by solid state NMR spectroscopy,
J. Phys. Chem. B 108, 18535-18546 (2004).
soujong@cheme.caltech.edu
L. Chen, M. J. Zhang, Y. Yue, C. H. Ye, and F. Deng
NMR and theoretical studies of boron-modified mordenite,
Microporous Mesoporous Mater. 76, 151-156 (2004).
dengf@wipm.ac.cn
D. Holland, A. C. Hannon, M. E. Smith, C. E. Johnson, M. F. Thomas, and A. M. Beesley
The role of Sb⁵⁺ in the structure of Sb₂O₃-B₂O₃ binary glasses-an NMR and Mössbauer spectroscopy study,
Solid-State NMR 26, 172-179 (2004).
d.holland@warwick.ac.uk
M. R. Hansen, T. Vosegaard, H. J. Jakobsen, and J. Skibsted
¹¹B chemical shift anisotropies in borates from ¹¹B MAS, MQMAS, and single-crystal NMR spectroscopy,
J. Phys. Chem. A 108, 586-594 (2004).
jskib@chem.au.dk
M. Edén and L. Frydman
Homonuclear NMR correlations between half-integer quadrupolar nuclei undergoing magic-angle spinning,
J. Phys. Chem. B 107, 14598-14611 (2003).
Lucio.Frydman@weizinann.ac.il
L. S. Du and J. F. Stebbins
Nature of silicon-boron mixing in sodium borosilicate glasses: A high-resolution ¹¹B and ¹⁷O NMR study,
J. Phys. Chem. B 107, 10063-10076 (2003).
lsdu@pangea.stanford.edu
M. A. M. Forgeron, D. L. Bryce, R. E. Wasylishen, and R. Rösler
A solid-state multinuclear magnetic resonance investigation of hexamethylborazine,
J. Phys. Chem. A 107, 726-735 (2003).
roderick.wasylishen@ualberta.ca
J. Grinshtein and L. Frydman
Solid state separated-local-field NMR spectroscopy on half-integer quadrupolar nuclei: Principles and applications to borane analysis,
J. Am. Chem. Soc. 125, 7451-7460 (2003).
lucio.frydman@weizmann.ac.il
K. Müller
Spin relaxation in isolated and coupled non-integer quadrupolar nuclei: Theory and application for I=3/2 nuclei,
Phys. Chem. Chem. Phys. 4, 5515-5523 (2002).
k.mueller@ipc.uni-stuttgart.de
L. van Wüllen and G. Schwering
¹¹B-MQMAS and ²⁹Si-{¹¹B} double-resonance NMR studies on the structure of binary B₂O₃-SiO₂ glasses,
Solid State NMR 21, 134-144 (2002).
wullen@jansen.mpi-stuttgart.mpg.de
S. Wi, J. W. Logan, D. Sakellariou, J. D. Walls, and A. Pines
Rotary resonance recoupling for half-integer quadrupolar nuclei in solid-state nuclear magnetic resonance spectroscopy,
J. Chem. Phys. 117, 7024-7033 (2002).
pines@cchem.berkeley.edu
R. W. Schurko, I. Hung, S. Schauff, C. L. B. Macdonald, and A. H. Cowley
Anisotropic ¹¹B and ¹³C NMR interaction tensors in decamethylcyclopentadienyl boron complexes,
J. Phys. Chem. A 106, 10096-10107 (2002).
K. Kanehashi and K. Saito
Structural analysis of boron compounds using ¹¹B-3QMAS solid state NMR,
J. Molec. Struct. 602-603, 105-113 (2002).
kanehasi@re.nsc.co.jp
J.-P. Amoureux and M. Pruski
Theoretical and experimental assessment of single- and multiple-quantum cross-polarization in solid state NMR,
Molec. Phys. 100, 1595-1613 (2002).
mpruski@iastate.edu
S. Kroeker and J. F. Stebbins
Three-coordinated Boron-11 chemical shifts in Borates,
Inorg. Chem. 40, 6239-6246 (2001).
Scott_Kroeker@UManitoba.ca
D. L. Bryce, R. E. Wasylishen, and M. Gee
Characterization of tricoordinate boron chemical shift tensors: definitive high-field solid-state NMR evidence for anisotropic boron shielding,
J. Phys. Chem. A 105, 3633-3640 (2001).
roderick.wasylishen@ualberta.ca
A. J. Woo, D.-Y. Han, and K. H. Yang
¹¹B nutation NMR study of powdered borosilicates,
Bull. Korean Chem. Soc. 19, 519-524 (1998).

Related bibliography

L. Regli, S. Bordiga, C. Lamberti, K. P. Lillerud, S. I. Zones, and A. Zecchinese
Effect of boron substitution in chabazite framework: IR studies on the acidity properties and reactivity towards methanol,
J. Phys. Chem. C 111, 2992-2999 (2007).
silvia.bordiga@unito.it
G. Kordas
HYSCORE spectroscopy in the borate glasses,
J. Non-Cryst. Solids 331, 122-127 (2003).
gkordas@ims.demokritos.gr

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