Reference for SPAM MQ-MAS

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SPAM MQ-MAS references

Below are provided some NMR references about MQ-MAS with SPAM applied to half-integer quadrupole spins. These references contain
(1) the pulse-sequence diagram,
(2) the coherence-transfer pathways,
(3) the phase-cycling,
(4) the receiver-phase relationship.

  1. Zhehong Gan, Peter L. Gor’kov, William W. Brey, Paul J. Sideris, and Clare P. Grey
    Enhancing MQMAS of low-γ nuclei by using a high B1 field balanced probe circuit, (1)(2)
    J. Magn. Reson. 200, 2-5 (2009).
    Abstract
  2. Takafumi Takahashi, Koji Kanehashi, Yuichi Shimoikeda, Takahiro Nemoto, and Koji Saito
    Practical comparison of sensitivity and resolution between STMAS and MQMAS for 27Al, (1)(2)(3)
    J. Magn. Reson. 198, 228-235 (2009).
    Abstract
  3. T. J. Ball and S. Wimperis
    Use of SPAM and FAM pulses in high-resolution MAS NMR spectroscopy of quadrupolar nuclei,
    J. Magn. Reson. 187, 343-351 (2007).
  4. J. W. Wiench, G. Tricot, L. Delevoye, J. Trebosc, J. Frye, L. Montagne, J.-P. Amoureux, and M. Pruski
    SPAM-MQ-HETCOR: an improved method for heteronuclear correlation spectroscopy between quadrupolar and spin-1/2 nuclei in solid-state NMR,
    Phys. Chem. Chem. Phys. 8, 144-150 (2006).
  5. J.-P. Amoureux, L. Delevoye, G. Fink, F. Taulelle, A. Flambard, and L. Montagne
    Implementing SPAM into STMAS: a net sensitivity improvement in high-resolution NMR of quadrupolar nuclei,
    J. Magn. Reson. 175, 285-299 (2005).
  6. J.-P. Amoureux, A. Flambard, L. Delevoye, and L. Montagne
    A very sensitive high-resolution NMR method for quadrupolar nuclei: SPAM-DQF-STMAS,
    Chem. Commun.3472-3474 (2005).
  7. N. Malicki, L. Mafra, A.-A. Quoineaud, J. Rocha, F. Thibault-Starzyk, and C. Fernandez
    Multiplex MQMAS NMR of quadrupolar nuclei, (1)(2)(3)
    Solid State Nucl. Magn. Reson. 28, 13-21 (2005).
  8. Z. H. Gan and H. T. Kwak
    Enhancing MQMAS sensitivity using signals from multiple coherence transfer pathways,
    J. Magn. Reson. 168, 346-351 (2004).

Solid-state NMR bibliography for:

Aluminum-27
Antimony-121/123
Arsenic-75
Barium-135/137
Beryllium-9
Bismuth-209
Boron-11
Bromine-79/81
Calcium-43
Cesium-133
Chlorine-35/37
Chromium-53
Cobalt-59
Copper-63/65
Deuterium-2
Gallium-69/71
Germanium-73
Gold-197
Hafnium-177/179
Indium-113/115
Iodine-127
Iridium-191/193
Krypton-83
Lanthanum-139
Lithium-7
Magnesium-25
Manganese-55
Mercury-201
Molybdenum-95/97
Neon-21
Nickel-61
Niobium-93
Nitrogen-14
Osmium-189
Oxygen-17
Palladium-105
Potassium-39/41
Rhenium-185/187
Rubidium-85/87
Ruthenium-99/101
Scandium-45
Sodium-23
Strontium-87
Sulfur-33
Tantalum-181
Titanium-47/49
Vanadium-51
Xenon-131
Zinc-67
Zirconium-91
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