NMR pulse sequence:
TRAPDOR references

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TRAnsfer of Population in DOuble Resonance references

Some NMR references about TRAPDOR pulse sequences involving half-integer quadrupole spins, (*) those containing the pulse-sequence diagram:

  • H. M. Kao, P. C. Chang, Y. W. Liao, L. P. Lee, and C. H. Chien
    Solid-state NMR characterization of the acid sites in cubic mesoporous Al-MCM-48 materials using trimethylphosphine oxide as a 31P NMR probe, (*)
    Microporous Mesoporous Mater. 114, 352-364 (2008).
  • J. G. Longstaffe, B. H. Chen, and Y. N. Huang
    Characterization of the amorphous phases formed during the synthesis of microporous material AlPO4-5,
    Microporous Mesoporous Mater. 98, 21-28 (2007).
  • G. M. Bowers, R. Ravella, S. Komarneni, and K. T. Mueller
    NMR study of strontium binding by a micaceous mineral, (*)
    J. Phys. Chem. B 116, 7159-7164 (2006).
  • A. Abraham, R. Prins, J. A. van-Bokhoven, E. R. H. van-Eck, and A. P. M. Kentgens
    Multinuclear solid-state high-resolution and 13C-{27Al} double-resonance magic-angle spinning NMR studies on aluminum alkoxides, (*)
    J. Phys. Chem. B 110, 6553-6560 (2006).
  • D. Zhou, J. Xu, J. H. Yu, L. Chen, F. Deng, and R. R. Xu
    Solid-state NMR spectroscopy of anionic framework aluminophosphates: A new method to determine the Al/P ratio,
    J. Phys. Chem. B 110, 2131-2137 (2006).
  • Y. N. Huang, Z. M. Yan, and R. Richer
    Characterization of BAPO- and SAPO-based mesoporous materials by solid-state NMR spectroscopy,
    Chem. Mater. 17, 6545-6554 (2005).
  • Q. Luo, J. Yang, W. Hu, M. Zhang, Y. Yue, C. Ye, and F. Deng
    Unambiguously distinguishing Si[3Si, 1Al] and Si[3Si, 1OH] structural units in zeolite by 1H/29Si/27Al triple resonance solid state NMR spectroscopy, (*)
    Solid State NMR 28, 9-13 (2005).
  • L. Peng, Y. Liu, N. Kim, J. E. Readman, and C. P. Grey
    Detection of Brønsted acid sites in zeolite HY with high-field 17O-MAS-NMR techniques, (*)
    Nature Mater. 4, 216-219 (2005).
  • Yining Huang and Zhimin Yan
    Probing the local environments of phosphorus in aluminophosphate-based mesostructured lamellar materials by solid-state NMR spectroscopy,
    J. Am. Chem. Soc. 127, 2731-2740 (2005).
  • S. Prabakar and K. T. Mueller
    Solid-state NMR investigations of sodium-cesium mixed-alkali phosphate glasses,
    J. Non-Cryst. Solids 349, 980-87 (2004).
  • M. D. Karra, K. J. Sutovich, and K. T. Mueller
    NMR characterization of Bronsted acid sites in faujasitic zeolites with use of perdeuterated trimethylphosphine oxide,
    J. Am. Chem. Soc. 124, 902-903 (2002).
  • M. Kalwei and H. Koller
    Quantitative comparison of REAPDOR and TRAPDOR experiments by numerical simulations and determination of H-Al distances in zeolites, (*)
    Solid State NMR 21, 145-157 (2002).
  • D. P. Lang, T. M. Alam, and D. N. Bencoe
    Solid-state 31P/27Al and 31P/23Na TRAPDOR NMR investigation of the phosphorus environments in sodium aluminophosphate glasses, (*)
    Chem. Mater. 13, 420-428 (2001).
  • R. D. Gougeon, P. R. Bodart, R. K. Harris, D. M. Kolonia, D. E. Petrakis, and P. J. Pomonis
    Solid-state NMR study of mesoporous phosphoro-vanado-aluminas, (*)
    Phys. Chem. Chem. Phys. 2, 5286-5292 (2000).
  • Qiang Zeng, Hanna Nekvasil, and C. P. Grey
    Proton environments in hydrous aluminosilicate glasses: a 1H MAS, 1H/27Al, and 1H/23Na TRAPDOR NMR study, (*)
    J. Phys. Chem. B 103, 7406-7415 (1999).
  • Haiming Liu, Hsien-Ming Kao, and Clare P. Grey
    1H MAS and 1H/27Al TRAPDOR NMR studies of oxygen-zeolite interactions at low temperatures: Probing Brønsted acid site accessibility,
    J. Phys. Chem. B 103, 4786-4796 (1999).
  • L. van Wüllen and M. Kalwei
    13C-27Al TRAPDOR and REDOR experiments for the detection of 13C-27Al dipolar interactions in solids, (*)
    J. Magn. Reson. 139, 250-257 (1999).
  • Leo van Wüllen
    1H-13C-27Al triple resonance transfer of populations in double resonance experiments for the detection of 13C-27Al dipolar interactions, (*)
    Solid State NMR 13, 123-127 (1998).
  • Leo van Wüllen
    Double resonance experiments in a single resonance probe: detecting 23Na-51V dipolar interactions in sodium vanadates, (*)
    Solid State NMR 10, 235-240 (1998).
  • F. Deng, G. Wang, Y. Du, C. Ye, Y. Kong, and X. Li
    1H MAS and 1H{23Na} double resonance NMR studies on the modification of surface hydroxyl groups of gamma-alumina by sodium,
    Solid State NMR 7, 281-290 (1997).
  • Hsien-Ming Kao and C. P. Grey
    Characterization of the Lewis acid sites in zeolite HY with the probe molecule trimethylphosphine, and 31P/27Al double resonance NMR, (*)
    Chem. Phys. Lett. 259, 459-464 (1996).
  • Hsien-Ming Kao and C. P. Grey
    Probing the Brønsted and Lewis acidity of zeolite HY: a 1H/27Al and 15N/27Al TRAPDOR NMR study of monomethylamine adsorbed on HY, (*)
    J. Phys. Chem. 100, 5105-5117 (1996).
  • E. R. H. van Eck, A. P. M. Kentgens, H. Kraus, and R. Prins
    A solid state double resonance NMR investigation of phosphorus-impregnated gamma-Al2O3, (*)
    J. Phys. Chem. 99, 16080-16086 (1995).
  • C. A. Fyfe, K. C. Wong-Moon, Y. Huang, H. Grondey, and K. T. Mueller
    Dipolar-based 27Al -> 29Si solid-state NMR connectivity experiments in zeolite molecular sieve frameworks, (*)
    J. Phys. Chem. 99, 8707-8716 (1995).
  • D. Freude
    Enhanced resolution in the 1H NMR spectra of zeolite H-ZSM-5 by heteronuclear dipolar-dephasing spin-echo MAS, (*)
    Chem. Phys. Lett. 235, 69-75 (1995).
  • C. P. Grey and A. J. Vega
    Determination of the quadrupole coupling constant of the invisible aluminum spins in zeolite HY with 1H/27Al TRAPDOR NMR, (*)
    J. Am. Chem. Soc. 117, 8232-8242 (1995).
  • M. A. Harmer and A. J. Vega
    Nuclear magnetic resonance study of a high-surface-area aluminum phosphate glass and its thermally reversible sol-gel precursor,
    Solid State NMR 5, 35-49 (1995).
  • L. W. Beck, J. L. White, and J. F. Haw
    1H{27Al} double-resonance experiments in solids: an unexpected observation in the 1H MAS spectrum of zeolite HZSM-5, (*)
    J. Am. Chem. Soc. 116, 9657-9661 (1994).
  • C. A. Fyfe, K. T. Mueller, H. Grondey, and K. C. Wong-Moon
    Solid-state double-resonance NMR experiments involving quadrupolar and spin 1/2 nuclei, (*)
    J. Phys. Chem. 97, 13484-13495 (1993).
  • C. P. Grey, W. S. Veeman, and A. J. Vega
    Rotational echo 14N/13C/1H triple resonance solid-state nuclear magnetic resonance: a probe of 13C-14N internuclear distances, (*)
    J. Chem. Phys. 98, 7711-7724 (1993).
  • C. P. Grey and W. S. Veeman
    The detection of weak heteronuclear coupling between spin 1 and spin 1/2 nuclei in MAS NMR; 14N/13C/1H triple resonance experiments,
    Chem. Phys. Lett. 192, 379-785 (1992).
  • E. R. H. van Eck, R. Janssen, W. E. J. R. Maas, and W. Veeman
    A novel application of nuclear spin-echo double-resonance to aluminophosphates and aluminosilicates, (*)
    Chem. Phys. Lett. 174, 428-432 (1990).


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