High power decoupling pulse program for topSpin2.1 operating system




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*** Outline ***


Code for Avance III spectrometers with topSpin2.1 operating system

;hpdec (TopSpin 2.0)

;acquisition on X with hp proton decoupling
;suitable for various types of decoupling

;Avance II+ version
;parameters:
;d1 : recycle delay
;d30 : =1s/cnst31-p4, for pidec12 and pidec13, pi-pulse decoupling
;d31 : =1s/cnst31, 1 rotor period
;p1 : X 90 degree pulse
;p5 : LG 360 degree pulse
;p10 : pulse length for phase modulated pulses (e.g PMLG, DUMBO)
;p22 : H 180 at power level pl13 (pidec)
;p29 : 5 - 10 us, to avoid exact rotor synchronisation
;pcpd2 : pulse length in decoupling sequence
;pl1 : X power level for excitation pulse
;pl2 : =119 dB, not used
;pl12 : power level for standard proton decoupling 
;pl13 : e.g. used in tppm13, pidec13, cw13, cwlg, cwlgs, lgs, xix13
;spnam1	: lgs-1, lgs-4 or pmlg-36
;l31 : number of rotor cycles for XiX (=3)
;cnst20 : proton RF field to calculate LG parameters
;cnst21 : =0, proton offset
;cnst22 : +ve Lee-Goldburg offset
;cnst23 : -ve Lee-Goldburg offset
;cnst24 : additional Lee-Goldburg offset
;cnst31 : spinning frequency
;cpdprg2 : sequence used for decoupling (tppm15, cw, xix12, etc.)
;zgoptns : -Dxix, -Dpidec, -Dlg

;$COMMENT=acquisition on X with proton decoupling, various decoupling schemes
;$CLASS=Solids
;$DIM=1D
;$TYPE=direct excitation
;$SUBTYPE=simple 1D

;$OWNER=Bruker
# ifdef xix
"pcpd=(1s*l31)/cnst31+p29"
# endif /* xix */

# ifdef pidec
"d30=1s/cnst31-p22"
# endif /* pidec */

# ifdef lg
#include <lgcalc.incl>
# endif
;cnst11 : to adjust t=0 for acquisition, if digmod = baseopt
"acqt0=1u*cnst11"

1 ze
2 d1 do:f2
  (p1 pl1 ph1):f1 (1u cpds2):f2
  go=2 ph31
  1m do:f2
  wr #0
exit

ph1= 0 2 1 3
ph31=0 2 1 3

References

  1. Paul Hogdkinson
    High-resolution 1H NMR spectroscopy of solids,
    Annu. Rep. Nucl. Magn. Reson. Spectrosc. 72, 185-223 (2011). Abstract, Google book
     
  2. Venus Singh Mithu, Subhradip Paul, Narayanan D. Kurur, and P. K. Madhu
    Heteronuclear dipolar decoupling in solid-state nuclear magnetic resonance under ultra-high magic-angle spinning,
    J. Magn. Reson. 209, 359-363 (2011).
    Abstract
     
  3. Ingo Scholz, Jacco D. van Beek, and Matthias Ernst
    Operator-based Floquet theory in solid-state NMR,
    Solid State Nucl. Magn. Reson. 37, 39-59 (2010).
    Abstract
     
  4. Subhradip Paul and P. K. Madhu
    On the choice of heteronuclear dipolar decoupling scheme in solid-state NMR,
    J. Magn. Reson. 207, 140-148 (2010).
    Abstract
     
  5. Subhradip Paul and P. K. Madhu
    Homonuclear dipolar decoupling in solid-state nuclear magnetic resonance under the regime of moderate to high magic-angle spinning frequencies: A status report,
    J. Indian Inst. Sci. 90, 69-86 (2010).
    Abstract
     
  6. Luís Mafra, Cristina Coelho, Renée Siegel, and João Rocha
    Assessing the performance of windowed 1H CRAMPS methods, on biological solids, at high-field and MAS up to 35 kHz,
    J. Magn. Reson. 197, 20-27 (2009).
    Abstract
     
  7. Anne Lesage
    Recent advances in solid-state NMR spectroscopy of spin I = 1/2 nuclei,
    Phys. Chem. Chem. Phys. 11, 6876-6891 (2009).
    Abstract
     
  8. Steven P. Brown
    Probing proton–proton proximities in the solid state,
    Prog. Nucl. Magn. Reson. Spectrosc. 50, 199-251 (2007).
    Abstract
     
  9. Paul Hodgkinson
    Heteronuclear decoupling in the NMR of solids,
    Prog. Nucl. Magn. Reson. Spectrosc. 46, 197-222 (2005).
    Abstract
     
  10. Steven P. Brown and Hans Wolfgang Spiess
    Advanced solid-state NMR methods for the elucidation of structure and dynamics of molecular, macromolecular, and supramolecular systems,
    Chem. Rev. 101, 4125-4155 (2001)
    Abstract
     
  11. Ingo Schnell and Hans Wolfgang Spiess
    High-resolution 1H NMR spectroscopy in the solid state: Very fast sample rotation and multiple-quantum coherences, in ADVANCES IN MAGNETIC RESONANCE
    J. Magn. Reson. 151, 153-227 (2001)
    Abstract
     

TPPM

  1. Subhradip Paul, Venus Singh Mithu, Narayanan D. Kurur, P. K. Madhu
    Efficient heteronuclear dipolar decoupling in solid-state nuclear magnetic resonance at rotary resonance conditions,
    J. Magn. Reson. 203, 199-202 (2010).
    Abstract
     
  2. K. Takegoshi, Jun Mizokami, and Takehiko Terao
    1H decoupling with third averaging in solid NMR,
    Chem. Phys. Lett. 341, 540-544 (2001).
    Abstract
     
  3. Zhehong Gan and R. R. Ernst
    Frequency- and phase-modulated heteronuclear decoupling in rotating solids,
    Solid State Nucl. Magn. Reson. 8, 153-159 (1997).
    Abstract
     
  4. Andrew E. Bennett, Chad M. Rienstra, Michèle Auger, K. V. Lakshmi, and Robert G. Griffin
    Heteronuclear decoupling in rotating solids,
    J. Chem. Phys. 103, 6951-6958 (1995).
    Abstract
     

SPINAL

  1. Gaël De Paëpe, Anne Lesage, and Lyndon Emsley
    The performance of phase modulated heteronuclear dipolar decoupling schemes in fast magic-angle-spinning nuclear magnetic resonance experiments,
    J. Chem. Phys. 119, 4833-4841 (2003).
    Abstract
     
  2. Thomas Braüniger, Philip Wormald, and Paul Hodgkinson
    Improved proton decoupling in NMR spectroscopy of crystalline solids using the SPINAL-64 sequence,
    Monatsh. Chem. 133, 1549-1554 (2002).
    Abstract
     
  3. B. M. Fung, A. K. Khitrin, and Konstantin Ermolaev
    An improved broadband decoupling sequence for liquid crystals and solids,
    J. Magn. Reson. 142, 97-101 (2000).
    Abstract
     

Pulse sequence symmetries

  1. Guangjin Hou, Si Yan, Shangjin Sun, Yun Han, In-Ja L. Byeon, Jinwoo Ahn, Jason Concel, Ago Samoson, Angela M. Gronenborn, and Tatyana Polenova
    Spin diffusion driven by R-symmetry sequences: Applications to homonuclear correlation spectroscopy in MAS NMR of biological and organic solids, (R2nν)
    J. Am. Chem. Soc. 133, 3943-3953 (2011).
    Abstract
     
  2. Subhradip Paul, Rajendra Singh Thakur, M. H. Levitt, and P. K. Madhu
    1H homonuclear dipolar decoupling using rotor-synchronised pulse sequences: Towards pure absorption phase spectra, (RNnN/2)
    J. Magn. Reson. 205, 269-275 (2010).
    Abstract
     
  3. Darren H. Brouwer and John A. Ripmeester
    Symmetry-based recoupling of proton chemical shift anisotropies in ultrahigh-field solid-state NMR, (R1825)
    J. Magn. Reson. 185, 173-178 (2007).
    Abstract
     
  4. Mattias Edén and Malcolm H. Levitt
    Pulse sequence symmetries in the nuclear magnetic resonance of spinning solids: Application to heteronuclear decoupling,
    J. Chem. Phys. 111, 1511-1519 (1999).
    Abstract
     

Decoupling Under Mind Boggling Optimisation DUMBO

  1. Amy L. Webber, Bénédicte Elena, John M. Griffin, Jonathan R. Yates, Tran N. Pham, Francesco Mauri, Chris J. Pickard, Ana M. Gil, Robin Stein, Anne Lesage, Lyndon Emsley, and Steven P. Brown
    Complete 1H resonance assignment of β-maltose from 1H-1H DQ-SQ CRAMPS and 1H (DQ-DUMBO)-13C SQ refocused INEPT 2D solid-state NMR spectra and first principles GIPAW calculations,
    Phys. Chem. Chem. Phys. 12, 6970-6983 (2010).
    Abstract
     
  2. Subhradip Paul, Rajendra Singh Thakur, Mithun Goswami, Andrea C. Sauerwein, Salvatore Mamone, Maria Concistrè, Hans Förster, Malcolm H. Levitt, and P. K. Madhu
    Supercycled homonuclear dipolar decoupling sequences in solid-state NMR,
    J. Magn. Reson. 197, 14-19 (2009).
    Abstract
     
  3. Elodie Salager, Robin S. Stein, Stefan Steuernagel, Anne Lesage, Bénédicte Elena, and Lyndon Emsley
    Enhanced sensitivity in high-resolution 1H solid-state NMR spectroscopy with DUMBO dipolar decoupling under ultra-fast MAS,
    Chem. Phys. Lett. 469, 336-341 (2009).
    Abstract
     
  4. John M. Griffin, Dave R. Martin, and Steven P. Brown
    Distinguishing anhydrous and hydrous forms of an active pharmaceutical ingredient in a tablet formulation using solid-state NMR spectroscopy,
    Angew. Chem. Int. Ed. 46, 8036-8038 (2007).
    Abstract
     
  5. Baohui Li, Lu Xu, Qiang Wu, Tiehong Chen, Pingchuan Sun, Qinghua Jin, Datong Ding, Xiaoliang Wang, Gi Xue, and An-Chang Shi
    Various types of hydrogen bonds, their temperature dependence and water-polymer interaction in hydrated poly(acrylic acid) as revealed by 1H solid-state NMR spectroscopy,
    Macromolecules 40, 5776-5786 (2007).
    Abstract
     
  6. Frédéric Blanc, Christophe Copéret, Jean Thivolle-Cazat, Jean-Marie Basset, Anne Lesage, Lyndon Emsley, Amritanshu Sinha, and Richard R. Schrock
    Surface versus molecular siloxy ligands in well-defined olefin metathesis catalysts: [{(RO)3SiO}Mo(=NAr)(=CHtBu)(CH2tBu)],
    Angew. Chem. Int. Ed. 45, 1216-1220 (2006).
    Abstract
     
  7. Bénédicte Elena, Anne Lesage, Stefan Steuernagel, Anja Böckmann, and Lyndon Emsley
    Proton to carbon-13 INEPT in solid-state NMR spectroscopy,
    J. Am. Chem. Soc. 127, 17296-17302 (2005).
    Abstract
     
  8. Steven P. Brown, Anne Lesage, Bénédicte Elena, and Lyndon Emsley
    Probing proton-proton proximities in the solid state: High-resolution two-dimensional 1H-1H double-quantum CRAMPS NMR spectroscopy,
    J. Am. Chem. Soc. 126, 13230-13231 (2004).
    Abstract
     
  9. Bénédicte Elena, Gaël de Paëpe, and Lyndon Emsley
    Direct spectral optimisation of proton-proton homonuclear dipolar decoupling in solid-state NMR,
    Chem. Phys. Lett. 398, 532-538 (2004).
    Abstract
     
  10. Gaël De Paëpe, Dimitris Sakellariou, Paul Hodgkinson, Sabine Hediger, and Lyndon Emsley
    Heteronuclear decoupling in NMR of Liquid Crystals using continuous phase modulation,
    Chem. Phys. Lett. 368, 511-522 (2003).
    Abstract
     
  11. Anne Lesage, Dimitris Sakellariou, Sabine Hediger, Bénédicte Eléna, Patrick Charmont, Stefan Steuernagel, and Lyndon Emsley
    Experimental aspects of proton NMR spectroscopy in solids using phase-modulated homonuclear dipolar decoupling,
    J. Magn. Reson. 163, 105-113 (2003).
    Abstract
     
  12. Dimitris Sakellariou, Anne Lesage, Paul Hodgkinson, and Lyndon Emsley
    Homonuclear dipolar decoupling in solid-state NMR using continuous phase modulation,
    Chem. Phys. Lett. 319, 253-260 (2000).
    Abstract
     
  13. D. P. Burum, M. Linder and R. R. Ernst
    Low-power multipulse line narrowing in solid-state NMR,
    J. Magn. Reson. 44, 173-188 (1981).
    Abstract
     

Lee-Goldburg

  1. Cristina Coelho, João Rocha, P. K. Madhu, and Luís Mafra
    Practical aspects of Lee-Goldburg based CRAMPS techniques for high-resolution 1H NMR spectroscopy in solids: Implementation and applications,
    J. Magn. Reson. 194, 264-282 (2008).
    Abstract
     
  2. Carl A. Michal, Simon P. Hastings, and Lik Hang Lee
    Two-photon Lee-Goldburg nuclear magnetic resonance: Simultaneous homonuclear decoupling and signal acquisition,
    J. Chem. Phys. 128, 052301/1-052301/8 (2008).
    Abstract
     
  3. Riqiang Fu, Changlin Tian, and Timothy A. Cross
    NMR spin locking of proton magnetization under a frequency-switched Lee-Goldburg pulse sequence,
    J. Magn. Reson. 154, 130-135 (2002).
    Abstract
     
  4. Anne Lesage and Lyndon Emsley
    Through-bond heteronuclear single-quantum correlation spectroscopy in solid-state NMR, and comparison to other through-bond and through-space experiments,
    J. Magn. Reson. 148, 449-454 (2001).
    Abstract
     
  5. Anne Lesage, Dimitris Sakellariou, Stefan Steuernagel, and Lyndon Emsley
    Carbon-proton chemical shift correlation in solid-state NMR by through-bond multiple-quantum spectroscopy,
    J. Am. Chem. Soc. 120, 13194-13201 (1998).
    Abstract
     
  6. Anne Lesage, Stefan Steuernagel, and Lyndon Emsley
    Carbon-13 spectral editing in solid-state NMR using heteronuclear scalar couplings,
    J. Am. Chem. Soc. 120, 7095-7100 (1998).
    Abstract
     
  7. B.-J. van Rossum, H. Förster, and H. J. M. de Groot
    High-field and high-speed CP-MAS 13C NMR heteronuclear dipolar-correlation spectroscopy of solids with frequency-switched Lee-Goldburg homonuclear decoupling,
    J. Magn. Reson. 124, 516-519 (1997).
    Abstract
     
  8. M. H. Levitt, A. C. Kolbert, A. Bielecki, and D. J. Ruben
    High-resolution 1H NMR in solids with frequency-switched multiple-pulse sequences,
    Solid State Nucl. Magn. Reson. 2, 151-163 (1993).
    Abstract
     
  9. A. Bielecki, A. C. Kolbert, H. J. M. De Groot, R. G. Griffin, and M. H. Levitt
    Frequency-switched Lee-Goldburg sequences in solids,
    in Advances in Magnetic Resonance, edited by Warren S. Warren (Academic Press, San Diego, vol. 14, 111-124, 1990).
    PDF file
     
  10. A. Bielecki, A. C. Kolbert, and M. H. Levitt
    Frequency-switched pulse sequences: Homonuclear decoupling and dilute spin NMR in solids,
    Chem. Phys. Lett. 155, 341-346 (1989).
    Abstract
     

CRAMPS

  1. D. Prato and P. W. Lamberti
    A note on Magnus formula,
    J. Chem. Phys. 106, 4640-4643 (1997).
    Abstract
     
  2. Thomas M. Barbara, Joel F. Martin, and Jon G. Wurl
    Phase transients in NMR probe circuits,
    J. Magn. Reson. 93, 497-508 (1991).
    Abstract
     
  3. Peter Jackson and Robin K. Harris
    A practical guide to combined rotation and multiple-pulse NMR spectroscopy of solids,
    Magn. Reson. Chem. 26, 1003-1011 (1988).
    Abstract
     
  4. A. K. Khitrin, V. V. Laiko, and B. N. Provotorov
    The influence of molecular motions on multipulse NMR spectra in solids,
    Phys. Stat. Sol. b 126, 481-486 (1984).
    Abstract
     
  5. S. Idziak and U. Haeberlen
    Design and construction of a high homogeneity rf coil for solid-state multiple-pulse NMR,
    J. Magn. Reson. 50, 281-288 (1982).
    Abstract
     
  6. D. P. Burum, M. Linder, and R. R. Ernst
    A new “tune-up” NMR pulse cycle for minimizing and characterizing phase transients,
    J. Magn. Reson. 43, 463-471 (1981).
    Abstract
     
  7. U. Haubenreisser and B. Schnabel
    Accurate phase adjustment for multiple pulse NMR of solids,
    J. Magn. Reson. 35, 175-184 (1979).
    Abstract
     
  8. R. G. Pembleton, L. M. Ryan, and B. C. Gerstein
    NMR probe for combined homonuclear multiple pulse decoupling and magic angle spinning,
    Rev. Sci. Instrum. 48, 1286-1289 (1977).
    Abstract
     
  9. B. C. Gerstein, C. Chow, R. G. Pembleton, and R. C. Wilson
    Utility of pulse nuclear magnetic resonance in studying protons in coals,
    J. Phys. Chem. 81, 565-570 (1977).
    Abstract
     
  10. C. R. Dybowski and R. W. Vaughan
    Motional phenomena and multiple pulse nuclear magnetic resonance. Nonisotropic motion in natural rubber,
    Macromolecules 8, 50-54 (1975).
    Abstract
     
  11. W-K. Rhim, D. D. Elleman, and R. W. Vaughan
    Enhanced resolution for solid state NMR,
    J. Chem. Phys. 58, 1772-1773 (1973).
    Abstract
     
  12. M. Mehring and J. S. Waugh
    Phase transients in pulsed NMR spectrometers,
    Rev. Sci. Instrum. 43, 649-653 (1972).
    Abstract
     
  13. Alexander Pines and John S. Waugh
    Quantitative aspects of coherent averaging. simple treatment of resonance offset processes in multiple-pulse NMR,
    J. Magn. Reson. 8, 354-365 (1972).
    Abstract
     
  14. M. Mehring and J. S. Waugh
    Magic-angle NMR experiments in solids,
    Phys. Rev. B 5, 3459-3471 (1972).
    Abstract
     
  15. U. Haeberlen and J. S. Waugh
    Coherent averaging effects in magnetic resonances,
    Phys. Rev. 175, 453-467 (1968).
    Abstract
     
  16. J. S. Waugh, L. M. Huber, and U. Haeberlen
    Approach to high-resolution nmr in solids,
    Phys. Rev. Lett. 20, 180-182 (1968).
    Abstract
     
  17. J. S. Waugh, C. H. Wang, L. M. Huber, and R. L. Vold
    Multiple-pulse NMR experiments,
    J. Chem. Phys. 48, 662-670 (1968).
    Abstract
     
  18. Moses Lee and Walter I. Goldburg
    Nuclear-Magnetic-Resonance line narrowing by a rotating rf field,
    Phys. Rev. 146, A1261-A1271 (1965).
    Abstract
     

PMLG

  1. Vega group web site
     
  2. Subhradip Paul, Rajendra Singh Thakur, M. H. Levitt, and P. K. Madhu
    1H homonuclear dipolar decoupling using rotor-synchronised pulse sequences: Towards pure absorption phase spectra, (RNnN/2)
    J. Magn. Reson. 205, 269-275 (2010).
    Abstract
     
  3. Kanmi Mao and Marek Pruski
    Homonuclear dipolar decoupling under fast MAS: Resolution patterns and simple optimization strategy,
    J. Magn. Reson. 203, 144-149 (2010).
    Abstract
     
  4. Simone Cavadini, Veronika Vitzthum, Simone Ulzega, Anuji Abraham, and Geoffrey Bodenhausen
    Line-narrowing in proton-detected nitrogen-14 NMR,
    J. Magn. Reson. 202, 57-63 (2010).
    Abstract
     
  5. Subhradip Paul, Rajendra Singh Thakur, Mithun Goswami, Andrea C. Sauerwein, Salvatore Mamone, Maria Concistrè, Hans Förster, Malcolm H. Levitt, and P. K. Madhu
    Supercycled homonuclear dipolar decoupling sequences in solid-state NMR,
    J. Magn. Reson. 197, 14-19 (2009).
    Abstract
     
  6. Michal Leskes, P. K. Madhu, and Shimon Vega
    Why does PMLG proton decoupling work at 65kHz MAS?,
    J. Magn. Reson. 199, 208-213 (2009).
    Abstract
     
  7. Michal Leskes, Stefan Steuernagel, Denis Schneider, P. K. Madhu, and Shimon Vega
    Homonuclear dipolar decoupling at magic-angle spinning frequencies up to 65 kHz in solid-state nuclear magnetic resonance,
    Chem. Phys. Lett. 466, 95-99 (2008).
    Abstract
     
  8. Michal Leskes, P. K. Madhu, and Shimon Vega
    Supercycled homonuclear dipolar decoupling in solid-state NMR: Toward cleaner 1H spectrum and higher spinning rates,
    J. Chem. Phys. 128, 052309/1-052309/11 (2008).
    Abstract
     
  9. Michal Leskes, P. K. Madhu, and Shimon Vega
    A broad-banded z-rotation windowed phase-modulated Lee-Goldburg pulse sequence for 1H spectroscopy in solid-state NMR,
    Chem. Phys. Lett. 447, 370-374 (2007).
    Abstract
     
  10. Michal Leskes, P. K. Madhu, and Shimon Vega
    Proton line narrowing in solid-state nuclear magnetic resonance: New insights from windowed phase-modulated Lee-Goldburg sequence,
    J. Chem. Phys. 125, 124506/1-124506/18 (2006).
    Abstract
     
  11. Veniamin Chevelkov, Kristina Rehbein, Anne Diehl, and Bernd Reif
    Ultrahigh resolution in proton solid-state NMR spectroscopy at high levels of deuteration,
    Angew. Chem. Int. Ed. 45, 3878-3881 (2006).
    Abstract
     
  12. Leon Bosman, P. K. Madhu, Shimon Vega, and Elena Vinogradov
    Improvement of homonuclear dipolar decoupling sequences in solid-state nuclear magnetic resonance utilising radiofrequency imperfections,
    J. Magn. Reson. 169, 39-48 (2004).
    Abstract
     
  13. Elena Vinogradov, P. K. Madhu, and Shimon Vega
    Strategies for high-resolution proton spectroscopy in solid-state NMR,
    in New Techniques in Solid-State NMR: Topics in Current Chemistry, J. Klinowski (Ed.),
    (Springer-Verlag, Heidelberg, pp 33-90, 2004).
    Google book
     
  14. Elena Vinogradov, P. K. Madhu, and Shimon Vega
    Proton spectroscopy in solid state nuclear magnetic resonance with windowed phase modulated Lee–Goldburg decoupling sequences,
    Chem. Phys. Lett. 354, 193-202 (2002).
    Abstract
     
  15. Elena Vinogradov, P. K. Madhu, and Shimon Vega
    Phase modulated Lee-Goldburg magic angle spinning proton nuclear magnetic resonance experiments in the solid state: A bimodal Floquet theoretical treatment,
    J. Chem. Phys. 115, 8983-9000 (2001).
    Abstract
     
  16. Elena Vinogradov, P. K. Madhu, and Shimon Vega
    A bimodal Floquet analysis of phase modulated Lee±Goldburg high resolution proton magic angle spinning NMR experiments,
    Chem. Phys. Lett. 329, 207-214 (2000).
    Abstract
     
  17. Elena Vinogradov, P. K. Madhu, and Shimon Vega
    High-resolution proton solid-state NMR spectroscopy by phase-modulated Lee-Goldburg experiment,
    Chem. Phys. Lett. 194, 443-450 (1999).
    Abstract
     

XiX

  1. Matthias Ernst, Ago Samoson, and Beat H. Meier
    Low-power XiX decoupling in MAS NMR experiments,
    J. Magn. Reson. 163, 332-339 (2003).
    Abstract
     
  2. Andreas Detken, Edme H. Hardy, Matthias Ernst, and Beat H. Meier
    Simple and efficient decoupling in magic-angle spinning solid-state NMR: the XiX scheme,
    Chem. Phys. Lett. 356, 298-304 (2002).
    Abstract
     
  3. P. Tekely, P. Palmas, and D. Canet
    Effect of proton spin exchange on the residual 13C MAS NMR linewidths. Phase-modulated irradiation for efficient heteronuclear decoupling in rapidly rotating solids,
    J. Magn. Reson. A 107, 129-133 (1994).
    Abstract
     

Phase-Inverted Supercycled Sequence for Attenuation of Rotary ResOnance PISSARRO

  1. Subhradip Paul, Venus Singh Mithu, Narayanan D. Kurur, P. K. Madhu
    Efficient heteronuclear dipolar decoupling in solid-state nuclear magnetic resonance at rotary resonance conditions,
    J. Magn. Reson. 203, 199-202 (2010).
    Abstract
     
  2. Markus Weingarth, Geoffrey Bodenhausen, and Piotr Tekely
    Low-power decoupling at high spinning frequencies in high static fields,
    J. Magn. Reson. 199, 238-241 (2009).
    Abstract
     
  3. Markus Weingarth, Piotr Tekely, and Geoffrey Bodenhausen
    Efficient heteronuclear decoupling by quenching rotary resonance in solid-state NMR,
    Chem. Phys. Lett. 466, 247-251 (2008).
    Abstract
     

Smooth amplitude modulation SAM

  1. Jean-Paul Amoureux, Bingwen Hu, Julien Trébosc, Qiang Wang, Olivier Lafon, and Feng Deng
    Homonuclear dipolar decoupling schemes for fast MAS,
    Solid State Nucl. Magn. Reson. 35, 19-24 (2009).
    Abstract
     
  2. Luís Mafra, José R. B. Gomes, Julien Trébosc, João Rocha, and Jean-Paul Amoureux
    1H-1H double-quantum CRAMPS NMR at very-fast MAS (νR = 35 kHz): A resolution enhancement method to probe 1H-1H proximities in solids,
    J. Magn. Reson. 196, 88-91 (2009).
    Abstract
     
  3. Olivier Lafon, Qiang Wang, Bingwen Hu, Julien Trébosc, Feng Deng, and Jean-Paul Amoureux
    Proton-proton homonuclear dipolar decoupling in solid-state NMR using rotor-synchronized z-rotation pulse sequences,
    J. Chem. Phys. 130, 014504/1-014504/13 (2009).
    Abstract
     
  4. Jean-Paul Amoureux, Bingwen Hu, and Julien Trébosc
    Enhanced resolution in proton solid-state NMR with very-fast MAS experiments,
    J. Magn. Reson. 193, 305-307 (2008).
    Abstract
     
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